Table 2. X-ray data-collection and refinement statistics.

Valeus in parentheses are for the highest resolution shell.

Resolution range (Å)	93.99–3.24 (3.35–3.24)
Space group	P212121
a, b, c (Å)	60.591, 165.037, 228.678
α, β, γ (°)	90, 90, 90
Total reflections	202345 (20961)
Unique reflections	37446 (3704)
Multiplicity	5.4 (5.7)
Completeness (%)	99.43 (99.78)
Mean I/σ(I)	7.87 (1.19)
Wilson B factor (Å2)	85.19
R merge	0.2136 (1.508)
R meas	0.2365 (1.661)
R p.i.m.	0.09988 (0.6879)
CC1/2	0.995 (0.651)
R work	0.245 (0.384)
R free	0.292 (0.408)
R.m.s.d., bond angles	0.002
R.m.s.d., angles	0.53
Ramachandran favored (%)	95.23
Ramachandran outliers (%)	0.07