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. 2022 Aug 30;78(Pt 9):330–337. doi: 10.1107/S2053230X22008317

Table 3. Structure solution and refinement.

Values in parentheses are for the outer shell.

Resolution range (Å) 45.12–2.43 (2.62–2.43)
Completeness (%) 99.2
σ Cutoff F > 1.35σ(F)
No. of reflections, working set 12625 (2467)
No. of reflections, test set 663 (132)
Final R cryst 0.205 (0.3330)
Final R free 0.268 (0.3800)
No. of non-H atoms
 Protein 1967
 RNA 800
 Ligand 24
 Water 60
R.m.s. deviations
 Bond lengths (Å) 0.010
 Angles (°) 1.443
Average B factors (Å2)
 Protein 83.49
 RNA 84.87
Ramachandran plot
 Most favoured (%) 94.63
 Allowed (%) 5.37
 Outliers (%) 0.00