| Xcalibur, Sapphire3 diffractometer | 6477 independent reflections |
| Radiation source: fine-focus sealed X-ray tube, Enhance (Mo) X-ray Source | 3049 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.104 |
| Detector resolution: 16.1827 pixels mm-1 | θmax = 30.0°, θmin = 3.0° |
| ω scans | h = −11→11 |
| Absorption correction: multi-scan (CrysAlisPro; Rigaku OD, 2018) | k = −25→24 |
| Tmin = 0.400, Tmax = 1.000 | l = −21→20 |
| 22680 measured reflections |
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