Table 3. Experimental details.
| Crystal data | |
| Chemical formula | C24H26N2O4S |
| M r | 438.53 |
| Crystal system, space group | Monoclinic, P21/n |
| Temperature (K) | 298 |
| a, b, c (Å) | 8.2608 (3), 17.9433 (7), 15.2470 (7) |
| β (°) | 100.626 (4) |
| V (Å3) | 2221.25 (16) |
| Z | 4 |
| Radiation type | Mo Kα |
| μ (mm−1) | 0.18 |
| Crystal size (mm) | 0.3 × 0.2 × 0.1 |
| Data collection | |
| Diffractometer | Xcalibur, Sapphire3 |
| Absorption correction | Multi-scan (CrysAlis PRO; Rigaku OD, 2018 ▸) |
| T min, T max | 0.400, 1.000 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 22680, 6477, 3049 |
| R int | 0.104 |
| (sin θ/λ)max (Å−1) | 0.703 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.077, 0.253, 1.04 |
| No. of reflections | 6477 |
| No. of parameters | 321 |
| No. of restraints | 9 |
| H-atom treatment | H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) | 0.33, −0.52 |