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. 2022 Feb 17;7(Pt 2):x220148. doi: 10.1107/S2414314622001481
Ni1—S2 2.1192 (6) C11—C12 1.383 (3)
Ni1—S3 2.1207 (7) C11—H11 0.9500
Ni1—S4 2.1261 (6) C12—C13 1.380 (3)
Ni1—S1 2.1277 (7) C13—C14 1.382 (3)
Cl1—C4 1.743 (3) C13—H13 0.9500
Cl2—C12 1.741 (2) C14—H14 0.9500
Cl3—C18 1.740 (3) C15—C20 1.400 (3)
Cl4—C26 1.733 (2) C15—C16 1.400 (3)
S1—C7 1.706 (2) C15—C21 1.479 (3)
S2—C8 1.704 (2) C16—C17 1.380 (4)
S3—C21 1.706 (2) C16—H16 0.9500
S4—C22 1.713 (2) C17—C18 1.387 (5)
C1—C2 1.393 (3) C17—H17 0.9500
C1—C6 1.402 (3) C18—C19 1.371 (4)
C1—C7 1.477 (3) C19—C20 1.379 (4)
C2—C3 1.381 (4) C19—H19 0.9500
C2—H2 0.9500 C20—H20 0.9500
C3—C4 1.378 (4) C21—C22 1.397 (3)
C3—H3 0.9500 C22—C23 1.473 (3)
C4—C5 1.376 (4) C23—C24 1.397 (3)
C5—C6 1.379 (4) C23—C28 1.398 (3)
C5—H5 0.9500 C24—C25 1.386 (3)
C6—H6 0.9500 C24—H24 0.9500
C7—C8 1.399 (3) C25—C26 1.381 (3)
C8—C9 1.480 (3) C25—H25 0.9500
C9—C10 1.394 (3) C26—C27 1.388 (3)
C9—C14 1.400 (3) C27—C28 1.386 (3)
C10—C11 1.387 (3) C27—H27 0.9500
C10—H10 0.9500 C28—H28 0.9500
S2—Ni1—S3 87.80 (2) C12—C13—H13 120.4
S2—Ni1—S4 174.64 (3) C14—C13—H13 120.4
S3—Ni1—S4 91.24 (2) C13—C14—C9 120.6 (2)
S2—Ni1—S1 91.15 (2) C13—C14—H14 119.7
S3—Ni1—S1 178.94 (2) C9—C14—H14 119.7
S4—Ni1—S1 89.82 (2) C20—C15—C16 118.6 (2)
C7—S1—Ni1 105.72 (8) C20—C15—C21 121.0 (2)
C8—S2—Ni1 105.67 (8) C16—C15—C21 120.4 (2)
C21—S3—Ni1 105.66 (8) C17—C16—C15 120.6 (3)
C22—S4—Ni1 105.76 (8) C17—C16—H16 119.7
C2—C1—C6 117.9 (2) C15—C16—H16 119.7
C2—C1—C7 121.3 (2) C16—C17—C18 119.1 (3)
C6—C1—C7 120.7 (2) C16—C17—H17 120.5
C3—C2—C1 121.3 (2) C18—C17—H17 120.5
C3—C2—H2 119.3 C19—C18—C17 121.6 (3)
C1—C2—H2 119.3 C19—C18—Cl3 119.3 (2)
C4—C3—C2 119.2 (2) C17—C18—Cl3 119.1 (2)
C4—C3—H3 120.4 C18—C19—C20 119.3 (3)
C2—C3—H3 120.4 C18—C19—H19 120.3
C5—C4—C3 121.1 (2) C20—C19—H19 120.3
C5—C4—Cl1 119.5 (2) C19—C20—C15 120.8 (3)
C3—C4—Cl1 119.4 (2) C19—C20—H20 119.6
C4—C5—C6 119.6 (2) C15—C20—H20 119.6
C4—C5—H5 120.2 C22—C21—C15 124.79 (19)
C6—C5—H5 120.2 C22—C21—S3 119.14 (17)
C5—C6—C1 120.9 (2) C15—C21—S3 116.05 (16)
C5—C6—H6 119.6 C21—C22—C23 124.3 (2)
C1—C6—H6 119.6 C21—C22—S4 118.07 (16)
C8—C7—C1 124.84 (19) C23—C22—S4 117.60 (17)
C8—C7—S1 118.29 (17) C24—C23—C28 118.3 (2)
C1—C7—S1 116.84 (16) C24—C23—C22 120.7 (2)
C7—C8—C9 125.3 (2) C28—C23—C22 120.95 (19)
C7—C8—S2 118.86 (16) C25—C24—C23 121.3 (2)
C9—C8—S2 115.76 (17) C25—C24—H24 119.4
C10—C9—C14 118.9 (2) C23—C24—H24 119.4
C10—C9—C8 120.74 (19) C26—C25—C24 118.9 (2)
C14—C9—C8 120.3 (2) C26—C25—H25 120.6
C11—C10—C9 120.8 (2) C24—C25—H25 120.6
C11—C10—H10 119.6 C25—C26—C27 121.5 (2)
C9—C10—H10 119.6 C25—C26—Cl4 119.58 (18)
C12—C11—C10 118.9 (2) C27—C26—Cl4 118.88 (18)
C12—C11—H11 120.5 C28—C27—C26 118.8 (2)
C10—C11—H11 120.5 C28—C27—H27 120.6
C13—C12—C11 121.6 (2) C26—C27—H27 120.6
C13—C12—Cl2 118.56 (18) C27—C28—C23 121.1 (2)
C11—C12—Cl2 119.87 (18) C27—C28—H28 119.4
C12—C13—C14 119.3 (2) C23—C28—H28 119.4
C6—C1—C2—C3 −0.5 (4) C20—C15—C16—C17 −1.7 (4)
C7—C1—C2—C3 −177.8 (2) C21—C15—C16—C17 −179.0 (2)
C1—C2—C3—C4 −0.6 (4) C15—C16—C17—C18 0.3 (4)
C2—C3—C4—C5 1.2 (4) C16—C17—C18—C19 0.9 (4)
C2—C3—C4—Cl1 −178.4 (2) C16—C17—C18—Cl3 −179.4 (2)
C3—C4—C5—C6 −0.6 (4) C17—C18—C19—C20 −0.6 (4)
Cl1—C4—C5—C6 179.0 (2) Cl3—C18—C19—C20 179.73 (19)
C4—C5—C6—C1 −0.5 (4) C18—C19—C20—C15 −0.9 (4)
C2—C1—C6—C5 1.1 (4) C16—C15—C20—C19 2.0 (3)
C7—C1—C6—C5 178.4 (2) C21—C15—C20—C19 179.3 (2)
C2—C1—C7—C8 −142.3 (2) C20—C15—C21—C22 44.4 (3)
C6—C1—C7—C8 40.5 (3) C16—C15—C21—C22 −138.4 (2)
C2—C1—C7—S1 39.8 (3) C20—C15—C21—S3 −133.8 (2)
C6—C1—C7—S1 −137.4 (2) C16—C15—C21—S3 43.5 (3)
Ni1—S1—C7—C8 −0.78 (19) Ni1—S3—C21—C22 −2.11 (19)
Ni1—S1—C7—C1 177.20 (14) Ni1—S3—C21—C15 176.18 (15)
C1—C7—C8—C9 10.5 (3) C15—C21—C22—C23 6.6 (3)
S1—C7—C8—C9 −171.64 (17) S3—C21—C22—C23 −175.30 (17)
C1—C7—C8—S2 −172.99 (17) C15—C21—C22—S4 −174.10 (17)
S1—C7—C8—S2 4.8 (3) S3—C21—C22—S4 4.0 (3)
Ni1—S2—C8—C7 −6.26 (19) Ni1—S4—C22—C21 −3.77 (19)
Ni1—S2—C8—C9 170.53 (14) Ni1—S4—C22—C23 175.60 (14)
C7—C8—C9—C10 51.3 (3) C21—C22—C23—C24 42.9 (3)
S2—C8—C9—C10 −125.3 (2) S4—C22—C23—C24 −136.43 (19)
C7—C8—C9—C14 −132.1 (2) C21—C22—C23—C28 −137.6 (2)
S2—C8—C9—C14 51.3 (3) S4—C22—C23—C28 43.1 (3)
C14—C9—C10—C11 −0.2 (3) C28—C23—C24—C25 2.5 (3)
C8—C9—C10—C11 176.4 (2) C22—C23—C24—C25 −178.0 (2)
C9—C10—C11—C12 1.3 (4) C23—C24—C25—C26 −0.7 (4)
C10—C11—C12—C13 −1.3 (4) C24—C25—C26—C27 −1.7 (4)
C10—C11—C12—Cl2 178.92 (18) C24—C25—C26—Cl4 178.84 (18)
C11—C12—C13—C14 0.2 (4) C25—C26—C27—C28 2.2 (4)
Cl2—C12—C13—C14 179.98 (18) Cl4—C26—C27—C28 −178.26 (18)
C12—C13—C14—C9 0.9 (3) C26—C27—C28—C23 −0.4 (3)
C10—C9—C14—C13 −0.9 (3) C24—C23—C28—C27 −1.9 (3)
C8—C9—C14—C13 −177.6 (2) C22—C23—C28—C27 178.5 (2)