| Bruker D8 QUEST PHOTON 3 diffractometer | 8009 independent reflections |
| Radiation source: fine-focus sealed tube | 5941 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.056 |
| Detector resolution: 7.3910 pixels mm-1 | θmax = 29.7°, θmin = 2.4° |
| φ and ω scans | h = −13→13 |
| Absorption correction: numerical (SADABS; Krause et al., 2015) | k = −15→15 |
| Tmin = 0.76, Tmax = 0.88 | l = −20→20 |
| 89629 measured reflections |