| Crystal data |
| Chemical formula |
[Ni(C14H8Cl2S2)2] |
|
M
r
|
681.16 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
170 |
|
a, b, c (Å) |
9.5487 (4), 11.4141 (4), 15.0254 (6) |
| α, β, γ (°) |
107.486 (2), 94.791 (2), 111.423 (2) |
|
V (Å3) |
1419.16 (10) |
|
Z
|
2 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
1.37 |
| Crystal size (mm) |
0.27 × 0.15 × 0.10 |
| |
| Data collection |
| Diffractometer |
Bruker D8 QUEST PHOTON 3 diffractometer |
| Absorption correction |
Numerical (SADABS; Krause et al., 2015 ▸) |
|
T
min, T
max
|
0.76, 0.88 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
89629, 8009, 5941 |
|
R
int
|
0.056 |
| (sin θ/λ)max (Å−1) |
0.696 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.040, 0.112, 1.03 |
| No. of reflections |
8009 |
| No. of parameters |
334 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
0.78, −0.45 |
