Table 2. Experimental details.
| Crystal data | |
| Chemical formula | C10H13N3O3P+·Cl− |
| M r | 289.65 |
| Crystal system, space group | Monoclinic, P21/c |
| Temperature (K) | 298 |
| a, b, c (Å) | 11.5857 (6), 7.0616 (4), 16.6118 (9) |
| β (°) | 108.222 (2) |
| V (Å3) | 1290.92 (12) |
| Z | 4 |
| Radiation type | Cu Kα |
| μ (mm−1) | 3.86 |
| Crystal size (mm) | 0.12 × 0.09 × 0.08 |
| Data collection | |
| Diffractometer | Bruker D8 Venture |
| Absorption correction | Multi-scan (SADABS; Bruker, 2016 ▸) |
| T min, T max | 0.524, 0.753 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 11621, 2268, 2048 |
| R int | 0.046 |
| (sin θ/λ)max (Å−1) | 0.596 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.042, 0.129, 1.11 |
| No. of reflections | 2268 |
| No. of parameters | 166 |
| H-atom treatment | H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) | 0.21, −0.34 |