Table 2. Experimental details.
| Crystal data | |
| Chemical formula | K2[Ag2(C16H16N2O8S4)]5.2H2O |
| M r | 880.17 |
| Crystal system, space group | Monoclinic, P21/c |
| Temperature (K) | 153 |
| a, b, c (Å) | 13.386 (3), 6.0085 (7), 17.843 (3) |
| β (°) | 108.657 (15) |
| V (Å3) | 1359.7 (4) |
| Z | 2 |
| Radiation type | Mo Kα |
| μ (mm−1) | 2.12 |
| Crystal size (mm) | 0.24 × 0.13 × 0.05 |
| Data collection | |
| Diffractometer | Stoe IPDS 2 |
| Absorption correction | Multi-scan (MULABS; Spek, 2020 ▸) |
| T min, T max | 0.611, 1.000 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 9305, 2316, 2088 |
| R int | 0.043 |
| (sin θ/λ)max (Å−1) | 0.591 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.048, 0.114, 1.17 |
| No. of reflections | 2316 |
| No. of parameters | 218 |
| H-atom treatment | H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) | 1.14, −1.10 |