| Nonius KappaCCD diffractometer | 2429 reflections with I > 3.0σ(I) |
| Radiation source: Enraf Nonius FR590 | Rint = 0.04 |
| Graphite monochromator | θmax = 28.7°, θmin = 2.1° |
| Detector resolution: 9 pixels mm-1 | h = −15→16 |
| φ & ω scans | k = −14→14 |
| 9132 measured reflections | l = −23→23 |
| 4563 independent reflections |
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