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. 2022 Mar 29;7(Pt 3):x220283. doi: 10.1107/S2414314622002838
C1—C2 1.506 (2) C10—C16 1.379 (2)
C1—H1 0.9600 C11—C12 1.379 (2)
C1—H9 0.9600 C11—C20 1.388 (2)
C1—H10 0.9600 C11—N1 1.430 (2)
C2—C18 1.382 (2) C12—C13 1.384 (2)
C2—C3 1.386 (3) C12—H4 0.9300
C3—C4 1.381 (2) C13—C14 1.372 (3)
C3—H11 0.9300 C13—H3 0.9300
C4—C5 1.392 (2) C14—C21 1.378 (3)
C4—H6 0.9300 C14—H2 0.9300
C5—C19 1.395 (2) C15—O1 1.2279 (18)
C5—C6 1.474 (2) C15—C16 1.446 (2)
C6—C7 1.333 (2) C16—C17 1.412 (2)
C6—H12 0.9300 C17—N2 1.311 (2)
C7—C15 1.502 (2) C17—H5 0.9300
C7—C8 1.514 (2) C18—C19 1.383 (2)
C8—C9 1.538 (2) C18—H8 0.9300
C8—H13 0.9700 C19—H7 0.9300
C8—H14 0.9700 C20—C21 1.383 (3)
C9—C10 1.4925 (19) C20—H18 0.9300
C9—H15 0.9700 C21—H17 0.9300
C9—H16 0.9700 N1—N2 1.3867 (17)
C10—N1 1.3535 (18)
C2—C1—H1 109.5 C16—C10—C9 123.85 (13)
C2—C1—H9 109.5 C12—C11—C20 120.41 (16)
H1—C1—H9 109.5 C12—C11—N1 120.27 (13)
C2—C1—H10 109.5 C20—C11—N1 119.30 (15)
H1—C1—H10 109.5 C11—C12—C13 119.73 (16)
H9—C1—H10 109.5 C11—C12—H4 120.1
C18—C2—C3 117.79 (15) C13—C12—H4 120.1
C18—C2—C1 121.21 (17) C14—C13—C12 120.38 (19)
C3—C2—C1 120.99 (17) C14—C13—H3 119.8
C4—C3—C2 121.26 (16) C12—C13—H3 119.8
C4—C3—H11 119.4 C13—C14—C21 119.64 (18)
C2—C3—H11 119.4 C13—C14—H2 120.2
C3—C4—C5 121.32 (16) C21—C14—H2 120.2
C3—C4—H6 119.3 O1—C15—C16 122.29 (13)
C5—C4—H6 119.3 O1—C15—C7 122.50 (14)
C4—C5—C19 117.09 (14) C16—C15—C7 115.20 (12)
C4—C5—C6 119.64 (14) C10—C16—C17 104.99 (13)
C19—C5—C6 123.27 (14) C10—C16—C15 122.98 (13)
C7—C6—C5 128.94 (14) C17—C16—C15 132.02 (14)
C7—C6—H12 115.5 N2—C17—C16 111.97 (14)
C5—C6—H12 115.5 N2—C17—H5 124.0
C6—C7—C15 118.02 (14) C16—C17—H5 124.0
C6—C7—C8 125.46 (13) C2—C18—C19 121.22 (16)
C15—C7—C8 116.51 (13) C2—C18—H8 119.4
C7—C8—C9 113.58 (13) C19—C18—H8 119.4
C7—C8—H13 108.8 C18—C19—C5 121.25 (15)
C9—C8—H13 108.8 C18—C19—H7 119.4
C7—C8—H14 108.8 C5—C19—H7 119.4
C9—C8—H14 108.8 C21—C20—C11 118.89 (19)
H13—C8—H14 107.7 C21—C20—H18 120.6
C10—C9—C8 107.83 (12) C11—C20—H18 120.6
C10—C9—H15 110.1 C14—C21—C20 120.94 (18)
C8—C9—H15 110.1 C14—C21—H17 119.5
C10—C9—H16 110.1 C20—C21—H17 119.5
C8—C9—H16 110.1 C10—N1—N2 111.28 (12)
H15—C9—H16 108.5 C10—N1—C11 130.21 (12)
N1—C10—C16 106.89 (12) N2—N1—C11 118.44 (12)
N1—C10—C9 129.20 (13) C17—N2—N1 104.86 (12)
C18—C2—C3—C4 0.6 (3) O1—C15—C16—C10 −168.78 (15)
C1—C2—C3—C4 −178.75 (18) C7—C15—C16—C10 10.8 (2)
C2—C3—C4—C5 1.8 (3) O1—C15—C16—C17 10.0 (3)
C3—C4—C5—C19 −2.7 (2) C7—C15—C16—C17 −170.40 (16)
C3—C4—C5—C6 177.62 (15) C10—C16—C17—N2 −0.38 (19)
C4—C5—C6—C7 −137.43 (18) C15—C16—C17—N2 −179.36 (16)
C19—C5—C6—C7 42.9 (3) C3—C2—C18—C19 −1.9 (3)
C5—C6—C7—C15 179.80 (15) C1—C2—C18—C19 177.42 (17)
C5—C6—C7—C8 0.7 (3) C2—C18—C19—C5 0.9 (3)
C6—C7—C8—C9 133.31 (17) C4—C5—C19—C18 1.3 (2)
C15—C7—C8—C9 −45.8 (2) C6—C5—C19—C18 −178.96 (15)
C7—C8—C9—C10 49.38 (18) C12—C11—C20—C21 0.1 (3)
C8—C9—C10—N1 150.39 (16) N1—C11—C20—C21 −178.39 (18)
C8—C9—C10—C16 −26.6 (2) C13—C14—C21—C20 0.0 (4)
C20—C11—C12—C13 0.4 (3) C11—C20—C21—C14 −0.3 (3)
N1—C11—C12—C13 178.88 (16) C16—C10—N1—N2 0.89 (17)
C11—C12—C13—C14 −0.7 (3) C9—C10—N1—N2 −176.49 (15)
C12—C13—C14—C21 0.5 (3) C16—C10—N1—C11 −176.18 (15)
C6—C7—C15—O1 14.8 (2) C9—C10—N1—C11 6.4 (3)
C8—C7—C15—O1 −166.01 (16) C12—C11—N1—C10 36.0 (2)
C6—C7—C15—C16 −164.78 (15) C20—C11—N1—C10 −145.48 (17)
C8—C7—C15—C16 14.4 (2) C12—C11—N1—N2 −140.90 (16)
N1—C10—C16—C17 −0.32 (17) C20—C11—N1—N2 37.6 (2)
C9—C10—C16—C17 177.24 (15) C16—C17—N2—N1 0.89 (19)
N1—C10—C16—C15 178.78 (14) C10—N1—N2—C17 −1.10 (18)
C9—C10—C16—C15 −3.7 (2) C11—N1—N2—C17 176.35 (14)