| Bruker APEXII CCD area detector diffractometer | 3431 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.038 |
| phi and ω scans | θmax = 28.8°, θmin = 1.9° |
| Absorption correction: multi-scan (SADABS; Bruker, 2003) | h = −28→40 |
| Tmin = 0.735, Tmax = 0.860 | k = −41→39 |
| 23938 measured reflections | l = −10→10 |
| 4924 independent reflections |