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. 2022 Mar 10;7(Pt 3):x220248. doi: 10.1107/S2414314622002486
F1—B1 1.44 (3) C7—C8 1.369 (8)
F2—B1 1.42 (3) C8—C9 1.444 (11)
F3—B1 1.52 (3) C8—C7A 1.271 (11)
F4—B1 1.248 (19) C8—C9A 1.442 (8)
F1A—B1A 1.26 (3) C9—H9 0.9300
F2A—B1A 1.28 (4) C9—C10 1.329 (12)
F3A—B1A 1.39 (2) C10—H10 0.9300
F4A—B1A 1.31 (3) C11—C12 1.387 (5)
N1—C1 1.319 (6) C11—C16 1.362 (5)
N1—C5 1.312 (7) C12—C13 1.411 (5)
N2—C6 1.307 (8) C12—C17 1.460 (6)
N2—C10 1.359 (11) C13—H13 0.9300
N2—C11 1.487 (4) C13—C14 1.356 (6)
N2—C6A 1.303 (11) C14—H14 0.9300
N2—C10A 1.382 (8) C14—C15 1.328 (6)
C1—H1 0.9300 C15—H15 0.9300
C1—C2 1.375 (6) C15—C16 1.405 (5)
C2—H2 0.9300 C16—H16 0.9300
C2—C3 1.381 (5) C17—H17A 0.9600
C3—C4 1.363 (5) C17—H17B 0.9600
C3—C8 1.489 (4) C17—H17C 0.9600
C4—H4 0.9300 C6A—C7A 1.393 (12)
C4—C5 1.376 (6) C6A—H6A 0.9300
C5—H5 0.9300 C7A—H7A 0.9300
C6—H6 0.9300 C9A—C10A 1.372 (9)
C6—C7 1.350 (9) C9A—H9A 0.9300
C7—H7 0.9300 C10A—H10A 0.9300
F2—B1—F1 106.1 (19) C7A—C8—C9A 118.0 (6)
F2—B1—F3 104.7 (18) C9A—C8—C3 119.5 (4)
F4—B1—F2 110 (2) C8—C9—H9 119.9
F4—B1—F1 114 (2) C10—C9—C8 120.1 (7)
F4—B1—F3 117 (2) C10—C9—H9 119.9
F1—B1—F3 104.4 (19) N2—C10—H10 119.4
F1A—B1A—F2A 122 (3) C9—C10—N2 121.1 (8)
F1A—B1A—F3A 103 (2) C9—C10—H10 119.4
F1A—B1A—F4A 108 (2) C12—C11—N2 119.2 (3)
F2A—B1A—F3A 105.7 (17) C16—C11—N2 118.2 (3)
F2A—B1A—F4A 112 (2) C16—C11—C12 122.6 (3)
F4A—B1A—F3A 105 (2) C11—C12—C13 116.3 (4)
C5—N1—C1 114.6 (4) C11—C12—C17 122.5 (3)
C6—N2—C10 119.8 (6) C13—C12—C17 121.2 (4)
C6—N2—C11 119.1 (4) C12—C13—H13 119.5
C10—N2—C11 119.7 (6) C14—C13—C12 121.1 (4)
C6A—N2—C11 121.7 (6) C14—C13—H13 119.5
C6A—N2—C10A 118.5 (6) C13—C14—H14 119.4
C10A—N2—C11 119.8 (4) C15—C14—C13 121.2 (4)
N1—C1—H1 117.0 C15—C14—H14 119.4
N1—C1—C2 125.9 (5) C14—C15—H15 119.6
C2—C1—H1 117.0 C14—C15—C16 120.7 (4)
C1—C2—H2 120.8 C16—C15—H15 119.6
C1—C2—C3 118.4 (4) C11—C16—C15 118.1 (4)
C3—C2—H2 120.8 C11—C16—H16 120.9
C2—C3—C8 121.5 (3) C15—C16—H16 120.9
C4—C3—C2 116.2 (3) C12—C17—H17A 109.5
C4—C3—C8 122.2 (3) C12—C17—H17B 109.5
C3—C4—H4 119.7 C12—C17—H17C 109.5
C3—C4—C5 120.5 (4) H17A—C17—H17B 109.5
C5—C4—H4 119.7 H17A—C17—H17C 109.5
N1—C5—C4 124.3 (4) H17B—C17—H17C 109.5
N1—C5—H5 117.9 C8—C7A—H7A 118.7
C4—C5—H5 117.9 C8—C7A—C6A 122.7 (8)
N2—C6—H6 119.8 N2—C6A—C7A 121.3 (9)
N2—C6—C7 120.4 (6) N2—C6A—H6A 119.4
C7—C6—H6 119.8 N2—C10A—H10A 119.6
C6—C7—H7 118.5 C8—C9A—H9A 121.0
C6—C7—C8 123.0 (6) C6A—C7A—H7A 118.7
C8—C7—H7 118.5 C7A—C6A—H6A 119.4
C7—C8—C3 122.6 (4) C9A—C10A—N2 120.8 (6)
C7—C8—C9 113.9 (5) C9A—C10A—H10A 119.6
C9—C8—C3 122.6 (5) C10A—C9A—C8 117.9 (6)
C7A—C8—C3 122.2 (5) C10A—C9A—H9A 121.0
N1—C1—C2—C3 −0.1 (6) C7—C8—C9—C10 −10.3 (10)
N2—C6—C7—C8 1.4 (12) C8—C3—C4—C5 178.2 (3)
N2—C11—C12—C13 179.8 (3) C8—C9—C10—N2 1.4 (11)
N2—C11—C12—C17 −2.1 (5) C8—C7A—C6A—N2 1.7 (11)
N2—C11—C16—C15 −179.9 (3) C10—N2—C6—C7 −11.3 (11)
N2—C10A—C9A—C8 4.7 (11) C10—N2—C11—C12 92.2 (6)
C1—N1—C5—C4 1.6 (7) C10—N2—C11—C16 −89.8 (6)
C1—C2—C3—C4 0.7 (5) C11—N2—C6—C7 −178.1 (6)
C1—C2—C3—C8 −177.6 (3) C11—N2—C10—C9 176.6 (6)
C2—C3—C4—C5 −0.1 (5) C11—N2—C6A—C7A 176.5 (5)
C2—C3—C8—C7 24.5 (6) C11—N2—C10A—C9A −179.9 (6)
C2—C3—C8—C9 −166.9 (6) C11—C12—C13—C14 −1.1 (5)
C2—C3—C8—C7A 171.8 (6) C12—C11—C16—C15 −1.9 (6)
C2—C3—C8—C9A −14.9 (6) C12—C13—C14—C15 0.4 (6)
C3—C4—C5—N1 −1.1 (7) C13—C14—C15—C16 −0.4 (6)
C3—C8—C9—C10 −179.9 (5) C14—C15—C16—C11 1.1 (6)
C3—C8—C7A—C6A −179.7 (5) C16—C11—C12—C13 1.9 (5)
C3—C8—C9A—C10A 176.6 (5) C16—C11—C12—C17 180.0 (4)
C4—C3—C8—C7 −153.7 (6) C17—C12—C13—C14 −179.2 (4)
C4—C3—C8—C9 14.9 (6) C7A—C8—C9A—C10A −9.8 (10)
C4—C3—C8—C7A −6.4 (7) C6A—N2—C11—C12 113.3 (6)
C4—C3—C8—C9A 166.9 (5) C6A—N2—C11—C16 −68.7 (6)
C5—N1—C1—C2 −1.0 (7) C6A—N2—C10A—C9A 3.6 (10)
C6—N2—C10—C9 9.9 (11) C10A—N2—C11—C12 −63.2 (6)
C6—N2—C11—C12 −101.0 (6) C10A—N2—C11—C16 114.9 (5)
C6—N2—C11—C16 77.0 (6) C10A—N2—C6A—C7A −7.0 (9)
C6—C7—C8—C3 178.7 (6) C9A—C8—C7A—C6A 6.9 (10)
C6—C7—C8—C9 9.2 (11)