| Refinement on F2 | Primary atom site location: dual |
| Least-squares matrix: full | Secondary atom site location: difference Fourier map |
| R[F2 > 2σ(F2)] = 0.108 | Hydrogen site location: inferred from neighbouring sites |
| wR(F2) = 0.378 | H-atom parameters constrained |
| S = 1.63 | w = 1/[σ2(Fo2) + (0.2P)2] where P = (Fo2 + 2Fc2)/3 |
| 2786 reflections | (Δ/σ)max < 0.001 |
| 240 parameters | Δρmax = 0.45 e Å−3 |
| 30 restraints | Δρmin = −0.24 e Å−3 |