| Crystal data |
| Chemical formula |
C17H15N2
+·BF4
−
|
|
M
r
|
334.12 |
| Crystal system, space group |
Monoclinic, P21/n
|
| Temperature (K) |
200 |
|
a, b, c (Å) |
11.4260 (5), 9.0735 (3), 15.5434 (5) |
| β (°) |
102.118 (4) |
|
V (Å3) |
1575.54 (10) |
|
Z
|
4 |
| Radiation type |
Cu Kα |
| μ (mm−1) |
1.00 |
| Crystal size (mm) |
0.10 × 0.09 × 0.01 |
| |
| Data collection |
| Diffractometer |
XtaLAB Synergy, Dualflex, HyPix |
| Absorption correction |
Gaussian (CrysAlis PRO; Rigaku OD, 2019 ▸) |
|
T
min, T
max
|
0.845, 1.000 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
16394, 2786, 2296 |
|
R
int
|
0.023 |
| (sin θ/λ)max (Å−1) |
0.595 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.108, 0.378, 1.63 |
| No. of reflections |
2786 |
| No. of parameters |
240 |
| No. of restraints |
30 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
0.45, −0.24 |
