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. 2022 Mar 31;7(Pt 3):x220332. doi: 10.1107/S2414314622003327
S1—C7A 1.733 (2) C10—C11 1.385 (3)
S1—C2 1.758 (2) C10—C15 1.401 (3)
C2—N3 1.308 (3) C11—C12 1.388 (3)
C2—C8 1.464 (3) C12—C13 1.405 (3)
N3—C3A 1.380 (3) C13—C14 1.377 (3)
C3A—C4 1.406 (3) C14—C15 1.409 (3)
C3A—C7A 1.411 (3) C15—C16 1.434 (3)
C4—C5 1.375 (3) C4—H4 0.9500
C5—C6 1.407 (3) C5—H5 0.9500
C6—C7 1.378 (3) C6—H6 0.9500
C7—C7A 1.396 (3) C7—H7 0.9500
C8—C16 1.357 (3) C11—H11 0.9500
C8—C9 1.470 (3) C12—H12 0.9500
C9—O2 1.210 (3) C13—H13 0.9500
C9—O1 1.365 (3) C14—H14 0.9500
C10—O1 1.379 (2) C16—H16 0.9500
C7A—S1—C2 88.87 (10) C14—C13—C12 120.1 (2)
N3—C2—C8 122.13 (19) C13—C14—C15 120.63 (19)
N3—C2—S1 115.63 (16) C10—C15—C14 117.67 (19)
C8—C2—S1 122.24 (15) C10—C15—C16 118.07 (19)
C2—N3—C3A 110.75 (18) C14—C15—C16 124.25 (19)
N3—C3A—C4 125.9 (2) C8—C16—C15 121.26 (19)
N3—C3A—C7A 115.15 (19) C9—O1—C10 122.61 (16)
C4—C3A—C7A 119.0 (2) C5—C4—H4 120.5
C5—C4—C3A 119.1 (2) C3A—C4—H4 120.5
C4—C5—C6 121.2 (2) C4—C5—H5 119.4
C7—C6—C5 120.9 (2) C6—C5—H5 119.4
C6—C7—C7A 118.1 (2) C7—C6—H6 119.5
C7—C7A—C3A 121.7 (2) C5—C6—H6 119.5
C7—C7A—S1 128.67 (17) C6—C7—H7 121.0
C3A—C7A—S1 109.57 (16) C7A—C7—H7 121.0
C16—C8—C2 121.80 (18) C10—C11—H11 120.8
C16—C8—C9 119.64 (19) C12—C11—H11 120.8
C2—C8—C9 118.56 (18) C11—C12—H12 119.7
O2—C9—O1 116.96 (18) C13—C12—H12 119.7
O2—C9—C8 125.2 (2) C14—C13—H13 119.9
O1—C9—C8 117.81 (18) C12—C13—H13 119.9
O1—C10—C11 116.83 (18) C13—C14—H14 119.7
O1—C10—C15 120.59 (19) C15—C14—H14 119.7
C11—C10—C15 122.58 (19) C8—C16—H16 119.4
C10—C11—C12 118.41 (19) C15—C16—H16 119.4
C11—C12—C13 120.6 (2)
C7A—S1—C2—N3 1.07 (17) C16—C8—C9—O2 179.9 (2)
C7A—S1—C2—C8 −178.49 (18) C2—C8—C9—O2 −0.2 (3)
C8—C2—N3—C3A 179.04 (18) C16—C8—C9—O1 0.2 (3)
S1—C2—N3—C3A −0.5 (2) C2—C8—C9—O1 −179.90 (17)
C2—N3—C3A—C4 179.1 (2) O1—C10—C11—C12 −178.97 (18)
C2—N3—C3A—C7A −0.5 (3) C15—C10—C11—C12 0.4 (3)
N3—C3A—C4—C5 −179.1 (2) C10—C11—C12—C13 −0.9 (3)
C7A—C3A—C4—C5 0.5 (3) C11—C12—C13—C14 0.7 (3)
C3A—C4—C5—C6 −1.1 (3) C12—C13—C14—C15 0.1 (3)
C4—C5—C6—C7 0.6 (3) O1—C10—C15—C14 179.76 (18)
C5—C6—C7—C7A 0.4 (3) C11—C10—C15—C14 0.5 (3)
C6—C7—C7A—C3A −1.0 (3) O1—C10—C15—C16 −1.3 (3)
C6—C7—C7A—S1 177.72 (17) C11—C10—C15—C16 179.42 (19)
N3—C3A—C7A—C7 −179.79 (19) C13—C14—C15—C10 −0.7 (3)
C4—C3A—C7A—C7 0.6 (3) C13—C14—C15—C16 −179.6 (2)
N3—C3A—C7A—S1 1.3 (2) C2—C8—C16—C15 −179.62 (19)
C4—C3A—C7A—S1 −178.36 (16) C9—C8—C16—C15 0.3 (3)
C2—S1—C7A—C7 179.9 (2) C10—C15—C16—C8 0.2 (3)
C2—S1—C7A—C3A −1.24 (16) C14—C15—C16—C8 179.1 (2)
N3—C2—C8—C16 −5.4 (3) O2—C9—O1—C10 179.04 (18)
S1—C2—C8—C16 174.10 (16) C8—C9—O1—C10 −1.2 (3)
N3—C2—C8—C9 174.66 (19) C11—C10—O1—C9 −178.83 (18)
S1—C2—C8—C9 −5.8 (3) C15—C10—O1—C9 1.8 (3)