Skip to main content
. 2022 Mar 17;7(Pt 3):x220277. doi: 10.1107/S2414314622002772
Geometry. All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes.
Refinement. All H atoms were located in difference maps and those on C were thereafter treated as riding in geometrically idealized positions with C—H distances 0.95 Å for phenyl and 0.98 Å for methyl. Coordinates of the N—H hydrogen atom were refined. Uiso(H) values were assigned as 1.2Ueq for the attached atom (1.5 for methyl).