| Crystal data |
| Chemical formula |
[Dy2(C7H6NO2)4Cl2(C12H8N2)2] |
|
M
r
|
1300.82 |
| Crystal system, space group |
Monoclinic, P21/c
|
| Temperature (K) |
296 |
|
a, b, c (Å) |
8.8922 (1), 21.5425 (3), 12.9887 (1) |
| β (°) |
101.755 (1) |
|
V (Å3) |
2435.94 (5) |
|
Z
|
2 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
3.22 |
| Crystal size (mm) |
0.22 × 0.20 × 0.19 |
| |
| Data collection |
| Diffractometer |
Bruker SAINT CCD area detector |
| Absorption correction |
Multi-scan (SADABS; Bruker, 2008 ▸) |
|
T
min, T
max
|
0.626, 0.746 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
16420, 4487, 3954 |
|
R
int
|
0.024 |
| (sin θ/λ)max (Å−1) |
0.606 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.021, 0.056, 1.01 |
| No. of reflections |
4487 |
| No. of parameters |
325 |
| No. of restraints |
1 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
0.59, −0.34 |
