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. 2022 Apr 12;7(Pt 4):x220380. doi: 10.1107/S2414314622003807
Bruker APEXI CCD diffractometer 6594 independent reflections
Radiation source: fine-focus sealed tube 6107 reflections with I > 2σ(I)
Graphite monochromator Rint = 0.023
Detector resolution: 8.3660 pixels mm-1 θmax = 27.1°, θmin = 2.2°
phi and ω scans h = −11→11
Absorption correction: multi-scan (SADABS; Bruker, 2014) k = −15→15
Tmin = 0.518, Tmax = 0.746 l = −17→18
19410 measured reflections