Bruker APEXI CCD diffractometer | 6594 independent reflections |
Radiation source: fine-focus sealed tube | 6107 reflections with I > 2σ(I) |
Graphite monochromator | Rint = 0.023 |
Detector resolution: 8.3660 pixels mm-1 | θmax = 27.1°, θmin = 2.2° |
phi and ω scans | h = −11→11 |
Absorption correction: multi-scan (SADABS; Bruker, 2014) | k = −15→15 |
Tmin = 0.518, Tmax = 0.746 | l = −17→18 |
19410 measured reflections |