O2—C13 | 1.2026 (19) | C5—H5A | 0.9700 |
O3—C13 | 1.310 (2) | C5—H5B | 0.9700 |
O3—H3 | 0.902 (10) | C5—C6 | 1.473 (2) |
O4—C16 | 1.3016 (19) | C6—C7 | 1.185 (2) |
O4—H4 | 0.914 (10) | C7—C8 | 1.467 (2) |
O5—C16 | 1.2092 (19) | C8—H8A | 0.9700 |
C15—H15 | 0.9300 | C8—H8B | 0.9700 |
C15—C14 | 1.316 (2) | C9—H9A | 0.9700 |
C15—C16 | 1.483 (2) | C9—H9B | 0.9700 |
C13—C14 | 1.480 (2) | C9—C10 | 1.515 (3) |
C14—H14 | 0.9300 | C10—H10A | 0.9700 |
O1—C1 | 1.2372 (19) | C10—H10B | 0.9700 |
N1—C1 | 1.3293 (19) | C10—C11 | 1.511 (3) |
N1—C4 | 1.451 (2) | C11—H11A | 0.9700 |
N1—C5 | 1.452 (2) | C11—H11B | 0.9700 |
N2—C8 | 1.486 (2) | C11—C12 | 1.509 (3) |
N2—C9 | 1.4833 (19) | C12—H12A | 0.9700 |
N2—C12 | 1.490 (2) | C12—H12B | 0.9700 |
N2—H2 | 0.908 (19) | O6—C17 | 1.270 (3) |
C2—H2A | 0.9700 | O7—C17 | 1.243 (2) |
C2—H2B | 0.9700 | C17—C18 | 1.492 (3) |
C2—C1 | 1.495 (2) | C18—C18i | 1.295 (4) |
C2—C3 | 1.510 (3) | C18—H18 | 0.9300 |
C3—H3A | 0.9700 | O6A—C17A | 1.273 (14) |
C3—H3B | 0.9700 | O7A—C17A | 1.222 (14) |
C3—C4 | 1.509 (3) | C17A—C18A | 1.502 (14) |
C4—H4A | 0.9700 | C18A—C18Ai | 1.25 (2) |
C4—H4B | 0.9700 | C18A—H18A | 0.9300 |
C13—O3—H3 | 108.7 (16) | H5A—C5—H5B | 107.9 |
C16—O4—H4 | 110.0 (15) | C6—C5—H5A | 109.3 |
C14—C15—H15 | 117.9 | C6—C5—H5B | 109.3 |
C14—C15—C16 | 124.13 (15) | C7—C6—C5 | 178.83 (17) |
C16—C15—H15 | 117.9 | C6—C7—C8 | 174.81 (17) |
O2—C13—O3 | 123.57 (15) | N2—C8—H8A | 108.7 |
O2—C13—C14 | 122.35 (15) | N2—C8—H8B | 108.7 |
O3—C13—C14 | 114.08 (14) | C7—C8—N2 | 114.07 (14) |
C15—C14—C13 | 123.90 (15) | C7—C8—H8A | 108.7 |
C15—C14—H14 | 118.1 | C7—C8—H8B | 108.7 |
C13—C14—H14 | 118.1 | H8A—C8—H8B | 107.6 |
O4—C16—C15 | 114.39 (13) | N2—C9—H9A | 111.2 |
O5—C16—O4 | 123.90 (15) | N2—C9—H9B | 111.2 |
O5—C16—C15 | 121.70 (15) | N2—C9—C10 | 102.94 (13) |
C1—N1—C4 | 114.58 (13) | H9A—C9—H9B | 109.1 |
C1—N1—C5 | 123.48 (13) | C10—C9—H9A | 111.2 |
C4—N1—C5 | 121.90 (13) | C10—C9—H9B | 111.2 |
C8—N2—C12 | 116.01 (13) | C9—C10—H10A | 110.5 |
C8—N2—H2 | 103.0 (11) | C9—C10—H10B | 110.5 |
C9—N2—C8 | 116.32 (12) | H10A—C10—H10B | 108.7 |
C9—N2—C12 | 104.70 (13) | C11—C10—C9 | 106.06 (15) |
C9—N2—H2 | 108.6 (11) | C11—C10—H10A | 110.5 |
C12—N2—H2 | 107.8 (11) | C11—C10—H10B | 110.5 |
H2A—C2—H2B | 108.8 | C10—C11—H11A | 110.5 |
C1—C2—H2A | 110.7 | C10—C11—H11B | 110.5 |
C1—C2—H2B | 110.7 | H11A—C11—H11B | 108.7 |
C1—C2—C3 | 105.11 (15) | C12—C11—C10 | 106.27 (15) |
C3—C2—H2A | 110.7 | C12—C11—H11A | 110.5 |
C3—C2—H2B | 110.7 | C12—C11—H11B | 110.5 |
O1—C1—N1 | 123.90 (15) | N2—C12—C11 | 103.58 (13) |
O1—C1—C2 | 126.98 (15) | N2—C12—H12A | 111.0 |
N1—C1—C2 | 109.11 (14) | N2—C12—H12B | 111.0 |
C2—C3—H3A | 110.4 | C11—C12—H12A | 111.0 |
C2—C3—H3B | 110.4 | C11—C12—H12B | 111.0 |
H3A—C3—H3B | 108.6 | H12A—C12—H12B | 109.0 |
C4—C3—C2 | 106.81 (15) | O6—C17—C18 | 116.8 (2) |
C4—C3—H3A | 110.4 | O7—C17—O6 | 123.1 (2) |
C4—C3—H3B | 110.4 | O7—C17—C18 | 120.1 (2) |
N1—C4—C3 | 104.08 (14) | C17—C18—H18 | 117.8 |
N1—C4—H4A | 110.9 | C18i—C18—C17 | 124.4 (2) |
N1—C4—H4B | 110.9 | C18i—C18—H18 | 117.8 |
C3—C4—H4A | 110.9 | O6A—C17A—C18A | 116.1 (16) |
C3—C4—H4B | 110.9 | O7A—C17A—O6A | 123.5 (16) |
H4A—C4—H4B | 109.0 | O7A—C17A—C18A | 119.4 (16) |
N1—C5—H5A | 109.3 | C17A—C18A—H18A | 114.6 |
N1—C5—H5B | 109.3 | C18Ai—C18A—C17A | 130.7 (16) |
N1—C5—C6 | 111.67 (13) | C18Ai—C18A—H18A | 114.6 |
O2—C13—C14—C15 | −159.84 (18) | C5—N1—C1—O1 | 2.9 (2) |
O3—C13—C14—C15 | 19.3 (2) | C5—N1—C1—C2 | −176.77 (14) |
C14—C15—C16—O4 | −8.4 (2) | C5—N1—C4—C3 | −179.65 (16) |
C14—C15—C16—O5 | 170.45 (18) | C8—N2—C9—C10 | −169.44 (14) |
C16—C15—C14—C13 | 179.50 (15) | C8—N2—C12—C11 | 168.12 (15) |
N2—C9—C10—C11 | 25.88 (19) | C9—N2—C8—C7 | 59.62 (19) |
C2—C3—C4—N1 | −4.8 (2) | C9—N2—C12—C11 | 38.48 (17) |
C1—N1—C4—C3 | 2.4 (2) | C9—C10—C11—C12 | −2.6 (2) |
C1—N1—C5—C6 | 109.44 (16) | C10—C11—C12—N2 | −21.6 (2) |
C1—C2—C3—C4 | 5.5 (2) | C12—N2—C8—C7 | −64.18 (19) |
C3—C2—C1—O1 | 176.15 (18) | C12—N2—C9—C10 | −39.98 (16) |
C3—C2—C1—N1 | −4.2 (2) | O6—C17—C18—C18i | −171.2 (3) |
C4—N1—C1—O1 | −179.16 (16) | O7—C17—C18—C18i | 7.4 (4) |
C4—N1—C1—C2 | 1.17 (19) | O6A—C17A—C18A—C18Ai | −1 (3) |
C4—N1—C5—C6 | −68.36 (19) | O7A—C17A—C18A—C18Ai | −169 (2) |