Table 1. Hydrogen-bond geometry (Å, °).
D—H⋯A | D—H | H⋯A | D⋯A | D—H⋯A |
---|---|---|---|---|
C14—H14⋯O5i | 0.93 | 2.65 | 3.498 (2) | 152 |
C3—H3B⋯O1i | 0.97 | 2.43 | 3.381 (3) | 166 |
C5—H5B⋯O2ii | 0.97 | 2.51 | 3.434 (2) | 159 |
C8—H8A⋯O4iii | 0.97 | 2.54 | 3.191 (2) | 125 |
C8—H8A⋯O6iii | 0.97 | 2.53 | 3.456 (3) | 161 |
C8—H8B⋯O5iv | 0.97 | 2.52 | 3.480 (2) | 173 |
C9—H9A⋯O6iv | 0.97 | 2.56 | 3.228 (3) | 126 |
C10—H10A⋯O5v | 0.97 | 2.66 | 3.624 (3) | 175 |
C11—H11A⋯O4vi | 0.97 | 2.64 | 3.553 (3) | 157 |
C12—H12B⋯O7vii | 0.97 | 2.68 | 3.399 (2) | 132 |
C12—H12B⋯O7A vii | 0.97 | 2.37 | 3.139 (15) | 135 |
O4—H4⋯O6 | 0.91 (1) | 1.58 (1) | 2.483 (2) | 167 (2) |
O3—H3⋯O1 | 0.90 (1) | 1.69 (1) | 2.5739 (16) | 167 (2) |
N2—H2⋯O6iv | 0.908 (19) | 2.554 (18) | 3.172 (3) | 125.8 (14) |
N2—H2⋯O7iv | 0.908 (19) | 1.809 (19) | 2.705 (2) | 168.3 (17) |
N2—H2⋯O6A iv | 0.908 (19) | 2.43 (3) | 3.131 (19) | 133.6 (15) |
N2—H2⋯O7A iv | 0.908 (19) | 1.61 (2) | 2.489 (15) | 161.7 (17) |
Symmetry codes: (i)
; (ii)
; (iii)
; (iv)
; (v)
; (vi)
; (vii)
.