Nb1—Cl1 | 2.457 (2) | C6B_b—H6D_b | 0.9900 |
Nb1—Cl4 | 2.457 (2) | C7B_b—H7C_b | 0.9900 |
Nb1—Cl3 | 2.460 (2) | C7B_b—H7D_b | 0.9900 |
Nb1—Cl2 | 2.464 (2) | O7—C9 | 1.423 (9) |
Nb1—I1 | 2.9312 (7) | O7—C12 | 1.43 (1) |
Nb1—Nb4 | 2.9367 (8) | C9—C10 | 1.50 (1) |
Nb1—Nb5 | 2.9367 (8) | C9—H9A | 0.9900 |
Nb1—Nb3 | 2.9394 (8) | C9—H9B | 0.9900 |
Nb1—Nb2 | 2.9424 (8) | C10—C11 | 1.50 (1) |
Nb2—O1 | 2.219 (5) | C10—H10A | 0.9900 |
Nb2—Cl9 | 2.457 (2) | C10—H10B | 0.9900 |
Nb2—Cl1 | 2.461 (2) | C11—C12 | 1.49 (1) |
Nb2—Cl5 | 2.461 (2) | C11—H11A | 0.9900 |
Nb2—Cl8 | 2.473 (2) | C11—H11B | 0.9900 |
Nb2—Nb3 | 2.8867 (7) | C12—H12A | 0.9900 |
Nb2—Nb5 | 2.9008 (8) | C12—H12B | 0.9900 |
Nb2—Nb6 | 2.9381 (8) | O8—C16 | 1.438 (9) |
Nb3—O2 | 2.233 (4) | O8—C13 | 1.455 (8) |
Nb3—Cl5 | 2.462 (2) | C13—C14 | 1.51 (1) |
Nb3—Cl10 | 2.464 (2) | C13—H13A | 0.9900 |
Nb3—Cl2 | 2.465 (2) | C13—H13B | 0.9900 |
Nb3—Cl6 | 2.470 (2) | C14—C15 | 1.51 (1) |
Nb3—Nb4 | 2.9029 (8) | C14—H14A | 0.9900 |
Nb3—Nb6 | 2.9418 (8) | C14—H14B | 0.9900 |
Nb4—O3 | 2.232 (5) | C15—C16 | 1.52 (1) |
Nb4—Cl3 | 2.462 (2) | C15—H15A | 0.9900 |
Nb4—Cl11 | 2.463 (2) | C15—H15B | 0.9900 |
Nb4—Cl6 | 2.467 (2) | C16—H16A | 0.9900 |
Nb4—Cl7 | 2.468 (2) | C16—H16B | 0.9900 |
Nb4—Nb5 | 2.8923 (8) | O9—C17 | 1.39 (1) |
Nb4—Nb6 | 2.9366 (8) | O9—C20 | 1.40 (1) |
Nb5—O4 | 2.209 (5) | C17—C18 | 1.42 (2) |
Nb5—Cl4 | 2.452 (2) | C17—H17A | 0.9900 |
Nb5—Cl12 | 2.461 (2) | C17—H17B | 0.9900 |
Nb5—Cl7 | 2.475 (2) | C18—C19 | 1.49 (2) |
Nb5—Cl8 | 2.476 (2) | C18—H18A | 0.9900 |
Nb5—Nb6 | 2.9352 (8) | C18—H18B | 0.9900 |
Nb6—Cl12 | 2.456 (2) | C19—C20 | 1.49 (1) |
Nb6—Cl9 | 2.457 (2) | C19—H19A | 0.9900 |
Nb6—Cl11 | 2.461 (2) | C19—H19B | 0.9900 |
Nb6—Cl10 | 2.461 (2) | C20—H20A | 0.9900 |
Nb6—I2 | 2.9563 (7) | C20—H20B | 0.9900 |
O1—H1A | 0.8498 | O10—C21 | 1.41 (1) |
O1—H1B | 0.8500 | O10—C24 | 1.46 (1) |
O2—H2A | 0.8499 | C21—C22 | 1.43 (2) |
O2—H2B | 0.8501 | C21—H21A | 0.9900 |
O3—H3A | 0.8505 | C21—H21B | 0.9900 |
O3—H3B | 0.8501 | C22—C23 | 1.50 (2) |
O4—H4A | 0.8500 | C22—H22A | 0.9900 |
O4—H4B | 0.8498 | C22—H22B | 0.9900 |
O5—C1 | 1.420 (9) | C23—C24 | 1.46 (1) |
O5—C4 | 1.447 (9) | C23—H23A | 0.9900 |
C1—C2 | 1.49 (1) | C23—H23B | 0.9900 |
C1—H1C | 0.9900 | C24—H24A | 0.9900 |
C1—H1D | 0.9900 | C24—H24B | 0.9900 |
C2—C3 | 1.51 (1) | O11—C25 | 1.43 (1) |
C2—H2C | 0.9900 | O11—C28 | 1.432 (9) |
C2—H2D | 0.9900 | C25—C26 | 1.46 (2) |
C3—C4 | 1.51 (1) | C25—H25A | 0.9900 |
C3—H3C | 0.9900 | C25—H25B | 0.9900 |
C3—H3D | 0.9900 | C26—C27 | 1.37 (2) |
C4—H4C | 0.9900 | C26—H26A | 0.9900 |
C4—H4D | 0.9900 | C26—H26B | 0.9900 |
O6A_a—C8A_a | 1.48 (3) | C27—C28 | 1.50 (1) |
O6A_a—C5A_a | 1.53 (6) | C27—H27A | 0.9900 |
C5A_a—C6A_a | 1.55 (7) | C27—H27B | 0.9900 |
C5A_a—H5A_a | 0.9900 | C28—H28A | 0.9900 |
C5A_a—H5B_a | 0.9900 | C28—H28B | 0.9900 |
C6A_a—C7A_a | 1.46 (8) | O12—C32 | 1.409 (9) |
C6A_a—H6A_a | 0.9900 | O12—C29 | 1.44 (1) |
C6A_a—H6B_a | 0.9900 | C29—C30 | 1.51 (1) |
C7A_a—C8A_a | 1.5 (1) | C29—H29A | 0.9900 |
C7A_a—H7A_a | 0.9900 | C29—H29B | 0.9900 |
C7A_a—H7B_a | 0.9900 | C30—C31 | 1.50 (1) |
C8A_a—H8A_a | 0.9900 | C30—H30A | 0.9900 |
C8A_a—H8B_a | 0.9900 | C30—H30B | 0.9900 |
O6B_b—C5B_b | 1.2 (1) | C31—C32 | 1.51 (1) |
C5B_b—C6B_b | 1.6 (1) | C31—H31A | 0.9900 |
C5B_b—H5C_b | 0.9900 | C31—H31B | 0.9900 |
C5B_b—H5D_b | 0.9900 | C32—H32A | 0.9900 |
C6B_b—C7B_b | 1.6 (1) | C32—H32B | 0.9900 |
C6B_b—H6C_b | 0.9900 | ||
Cl1—Nb1—Cl4 | 88.15 (6) | Nb2—O1—H1A | 126.4 |
Cl1—Nb1—Cl3 | 164.99 (6) | Nb2—O1—H1B | 135.5 |
Cl4—Nb1—Cl3 | 89.96 (6) | H1A—O1—H1B | 91.8 |
Cl1—Nb1—Cl2 | 88.73 (6) | Nb3—O2—H2A | 109.8 |
Cl4—Nb1—Cl2 | 165.04 (6) | Nb3—O2—H2B | 127.2 |
Cl3—Nb1—Cl2 | 89.28 (6) | H2A—O2—H2B | 103.6 |
Cl1—Nb1—I1 | 82.67 (4) | Nb4—O3—H3A | 109.8 |
Cl4—Nb1—I1 | 81.57 (4) | Nb4—O3—H3B | 126.8 |
Cl3—Nb1—I1 | 82.32 (4) | H3A—O3—H3B | 108.6 |
Cl2—Nb1—I1 | 83.52 (4) | Nb5—O4—H4A | 109.4 |
Cl1—Nb1—Nb4 | 141.61 (5) | Nb5—O4—H4B | 109.3 |
Cl4—Nb1—Nb4 | 96.11 (4) | H4A—O4—H4B | 109.5 |
Cl3—Nb1—Nb4 | 53.40 (4) | C1—O5—C4 | 109.5 (6) |
Cl2—Nb1—Nb4 | 95.42 (4) | O5—C1—C2 | 107.2 (7) |
I1—Nb1—Nb4 | 135.71 (2) | O5—C1—H1C | 110.3 |
Cl1—Nb1—Nb5 | 95.59 (4) | C2—C1—H1C | 110.3 |
Cl4—Nb1—Nb5 | 53.17 (4) | O5—C1—H1D | 110.3 |
Cl3—Nb1—Nb5 | 95.17 (4) | C2—C1—H1D | 110.3 |
Cl2—Nb1—Nb5 | 141.75 (4) | H1C—C1—H1D | 108.5 |
I1—Nb1—Nb5 | 134.73 (2) | C1—C2—C3 | 103.0 (6) |
Nb4—Nb1—Nb5 | 59.00 (2) | C1—C2—H2C | 111.2 |
Cl1—Nb1—Nb3 | 94.90 (4) | C3—C2—H2C | 111.2 |
Cl4—Nb1—Nb3 | 141.48 (4) | C1—C2—H2D | 111.2 |
Cl3—Nb1—Nb3 | 95.84 (4) | C3—C2—H2D | 111.2 |
Cl2—Nb1—Nb3 | 53.40 (4) | H2C—C2—H2D | 109.1 |
I1—Nb1—Nb3 | 136.92 (2) | C4—C3—C2 | 103.2 (6) |
Nb4—Nb1—Nb3 | 59.21 (2) | C4—C3—H3C | 111.1 |
Nb5—Nb1—Nb3 | 88.35 (2) | C2—C3—H3C | 111.1 |
Cl1—Nb1—Nb2 | 53.30 (4) | C4—C3—H3D | 111.1 |
Cl4—Nb1—Nb2 | 94.48 (4) | C2—C3—H3D | 111.1 |
Cl3—Nb1—Nb2 | 141.71 (4) | H3C—C3—H3D | 109.1 |
Cl2—Nb1—Nb2 | 95.36 (4) | O5—C4—C3 | 106.2 (6) |
I1—Nb1—Nb2 | 135.96 (2) | O5—C4—H4C | 110.5 |
Nb4—Nb1—Nb2 | 88.31 (2) | C3—C4—H4C | 110.5 |
Nb5—Nb1—Nb2 | 59.13 (2) | O5—C4—H4D | 110.5 |
Nb3—Nb1—Nb2 | 58.78 (2) | C3—C4—H4D | 110.5 |
O1—Nb2—Cl9 | 80.9 (1) | H4C—C4—H4D | 108.7 |
O1—Nb2—Cl1 | 81.0 (1) | C8A_a—O6A_a—C5A_a | 107 (3) |
Cl9—Nb2—Cl1 | 161.91 (6) | O6A_a—C5A_a—C6A_a | 99 (3) |
O1—Nb2—Cl5 | 79.4 (1) | O6A_a—C5A_a—H5A_a | 112.0 |
Cl9—Nb2—Cl5 | 89.21 (6) | C6A_a—C5A_a—H5A_a | 112.0 |
Cl1—Nb2—Cl5 | 88.78 (6) | O6A_a—C5A_a—H5B_a | 112.0 |
O1—Nb2—Cl8 | 82.3 (1) | C6A_a—C5A_a—H5B_a | 112.0 |
Cl9—Nb2—Cl8 | 86.65 (6) | H5A_a—C5A_a—H5B_a | 109.7 |
Cl1—Nb2—Cl8 | 89.63 (6) | C7A_a—C6A_a—C5A_a | 105 (4) |
Cl5—Nb2—Cl8 | 161.62 (6) | C7A_a—C6A_a—H6A_a | 110.7 |
O1—Nb2—Nb3 | 133.5 (1) | C5A_a—C6A_a—H6A_a | 110.7 |
Cl9—Nb2—Nb3 | 97.19 (4) | C7A_a—C6A_a—H6B_a | 110.7 |
Cl1—Nb2—Nb3 | 96.17 (4) | C5A_a—C6A_a—H6B_a | 110.7 |
Cl5—Nb2—Nb3 | 54.11 (4) | H6A_a—C6A_a—H6B_a | 108.8 |
Cl8—Nb2—Nb3 | 144.22 (4) | C6A_a—C7A_a—C8A_a | 102 (5) |
O1—Nb2—Nb5 | 136.4 (1) | C6A_a—C7A_a—H7A_a | 111.4 |
Cl9—Nb2—Nb5 | 95.69 (4) | C8A_a—C7A_a—H7A_a | 111.4 |
Cl1—Nb2—Nb5 | 96.44 (4) | C6A_a—C7A_a—H7B_a | 111.4 |
Cl5—Nb2—Nb5 | 144.18 (4) | C8A_a—C7A_a—H7B_a | 111.4 |
Cl8—Nb2—Nb5 | 54.17 (4) | H7A_a—C7A_a—H7B_a | 109.3 |
Nb3—Nb2—Nb5 | 90.07 (2) | O6A_a—C8A_a—C7A_a | 108 (3) |
O1—Nb2—Nb6 | 134.2 (1) | O6A_a—C8A_a—H8A_a | 110.2 |
Cl9—Nb2—Nb6 | 53.29 (4) | C7A_a—C8A_a—H8A_a | 110.2 |
Cl1—Nb2—Nb6 | 144.78 (4) | O6A_a—C8A_a—H8B_a | 110.2 |
Cl5—Nb2—Nb6 | 96.26 (4) | C7A_a—C8A_a—H8B_a | 110.2 |
Cl8—Nb2—Nb6 | 95.58 (4) | H8A_a—C8A_a—H8B_a | 108.5 |
Nb3—Nb2—Nb6 | 60.66 (2) | O6B_b—C5B_b—C6B_b | 109 (8) |
Nb5—Nb2—Nb6 | 60.35 (2) | O6B_b—C5B_b—H5C_b | 109.9 |
O1—Nb2—Nb1 | 134.2 (1) | C6B_b—C5B_b—H5C_b | 109.9 |
Cl9—Nb2—Nb1 | 144.85 (4) | O6B_b—C5B_b—H5D_b | 109.9 |
Cl1—Nb2—Nb1 | 53.20 (4) | C6B_b—C5B_b—H5D_b | 109.9 |
Cl5—Nb2—Nb1 | 96.78 (4) | H5C_b—C5B_b—H5D_b | 108.3 |
Cl8—Nb2—Nb1 | 96.90 (5) | C7B_b—C6B_b—C5B_b | 91 (7) |
Nb3—Nb2—Nb1 | 60.56 (2) | C7B_b—C6B_b—H6C_b | 113.5 |
Nb5—Nb2—Nb1 | 60.34 (2) | C5B_b—C6B_b—H6C_b | 113.5 |
Nb6—Nb2—Nb1 | 91.58 (2) | C7B_b—C6B_b—H6D_b | 113.5 |
O2—Nb3—Cl5 | 80.2 (1) | C5B_b—C6B_b—H6D_b | 113.5 |
O2—Nb3—Cl10 | 81.6 (1) | H6C_b—C6B_b—H6D_b | 110.8 |
Cl5—Nb3—Cl10 | 87.84 (6) | C6B_b—C7B_b—H7C_b | 111.0 |
O2—Nb3—Cl2 | 80.1 (1) | C6B_b—C7B_b—H7D_b | 111.0 |
Cl5—Nb3—Cl2 | 89.33 (6) | H7C_b—C7B_b—H7D_b | 109.0 |
Cl10—Nb3—Cl2 | 161.77 (5) | C9—O7—C12 | 108.6 (6) |
O2—Nb3—Cl6 | 81.7 (1) | O7—C9—C10 | 106.2 (7) |
Cl5—Nb3—Cl6 | 161.93 (6) | O7—C9—H9A | 110.5 |
Cl10—Nb3—Cl6 | 89.20 (5) | C10—C9—H9A | 110.5 |
Cl2—Nb3—Cl6 | 87.92 (6) | O7—C9—H9B | 110.5 |
O2—Nb3—Nb2 | 134.3 (1) | C10—C9—H9B | 110.5 |
Cl5—Nb3—Nb2 | 54.08 (4) | H9A—C9—H9B | 108.7 |
Cl10—Nb3—Nb2 | 96.13 (4) | C11—C10—C9 | 104.8 (7) |
Cl2—Nb3—Nb2 | 96.76 (4) | C11—C10—H10A | 110.8 |
Cl6—Nb3—Nb2 | 143.99 (4) | C9—C10—H10A | 110.8 |
O2—Nb3—Nb4 | 135.6 (1) | C11—C10—H10B | 110.8 |
Cl5—Nb3—Nb4 | 144.11 (4) | C9—C10—H10B | 110.8 |
Cl10—Nb3—Nb4 | 96.56 (4) | H10A—C10—H10B | 108.9 |
Cl2—Nb3—Nb4 | 96.26 (4) | C12—C11—C10 | 103.5 (8) |
Cl6—Nb3—Nb4 | 53.95 (4) | C12—C11—H11A | 111.1 |
Nb2—Nb3—Nb4 | 90.04 (2) | C10—C11—H11A | 111.1 |
O2—Nb3—Nb1 | 133.5 (1) | C12—C11—H11B | 111.1 |
Cl5—Nb3—Nb1 | 96.83 (4) | C10—C11—H11B | 111.1 |
Cl10—Nb3—Nb1 | 144.85 (4) | H11A—C11—H11B | 109.0 |
Cl2—Nb3—Nb1 | 53.39 (4) | O7—C12—C11 | 103.1 (7) |
Cl6—Nb3—Nb1 | 95.83 (4) | O7—C12—H12A | 111.2 |
Nb2—Nb3—Nb1 | 60.66 (2) | C11—C12—H12A | 111.2 |
Nb4—Nb3—Nb1 | 60.35 (2) | O7—C12—H12B | 111.2 |
O2—Nb3—Nb6 | 134.9 (1) | C11—C12—H12B | 111.2 |
Cl5—Nb3—Nb6 | 96.15 (4) | H12A—C12—H12B | 109.1 |
Cl10—Nb3—Nb6 | 53.28 (4) | C16—O8—C13 | 109.3 (6) |
Cl2—Nb3—Nb6 | 144.95 (4) | O8—C13—C14 | 105.6 (6) |
Cl6—Nb3—Nb6 | 96.33 (4) | O8—C13—H13A | 110.6 |
Nb2—Nb3—Nb6 | 60.53 (2) | C14—C13—H13A | 110.6 |
Nb4—Nb3—Nb6 | 60.32 (2) | O8—C13—H13B | 110.6 |
Nb1—Nb3—Nb6 | 91.56 (2) | C14—C13—H13B | 110.6 |
O3—Nb4—Cl3 | 81.6 (1) | H13A—C13—H13B | 108.7 |
O3—Nb4—Cl11 | 80.0 (1) | C13—C14—C15 | 102.3 (7) |
Cl3—Nb4—Cl11 | 161.58 (6) | C13—C14—H14A | 111.3 |
O3—Nb4—Cl6 | 81.8 (1) | C15—C14—H14A | 111.3 |
Cl3—Nb4—Cl6 | 88.54 (6) | C13—C14—H14B | 111.3 |
Cl11—Nb4—Cl6 | 88.29 (6) | C15—C14—H14B | 111.3 |
O3—Nb4—Cl7 | 79.9 (1) | H14A—C14—H14B | 109.2 |
Cl3—Nb4—Cl7 | 88.21 (6) | C14—C15—C16 | 102.1 (7) |
Cl11—Nb4—Cl7 | 89.13 (6) | C14—C15—H15A | 111.3 |
Cl6—Nb4—Cl7 | 161.75 (6) | C16—C15—H15A | 111.3 |
O3—Nb4—Nb5 | 134.2 (1) | C14—C15—H15B | 111.3 |
Cl3—Nb4—Nb5 | 96.25 (4) | C16—C15—H15B | 111.3 |
Cl11—Nb4—Nb5 | 96.97 (4) | H15A—C15—H15B | 109.2 |
Cl6—Nb4—Nb5 | 143.93 (4) | O8—C16—C15 | 105.7 (6) |
Cl7—Nb4—Nb5 | 54.31 (4) | O8—C16—H16A | 110.6 |
O3—Nb4—Nb3 | 135.8 (1) | C15—C16—H16A | 110.6 |
Cl3—Nb4—Nb3 | 96.72 (4) | O8—C16—H16B | 110.6 |
Cl11—Nb4—Nb3 | 96.07 (4) | C15—C16—H16B | 110.6 |
Cl6—Nb4—Nb3 | 54.02 (4) | H16A—C16—H16B | 108.7 |
Cl7—Nb4—Nb3 | 144.23 (4) | C17—O9—C20 | 109.7 (8) |
Nb5—Nb4—Nb3 | 89.92 (2) | O9—C17—C18 | 110 (1) |
O3—Nb4—Nb6 | 133.4 (1) | O9—C17—H17A | 109.6 |
Cl3—Nb4—Nb6 | 145.05 (4) | C18—C17—H17A | 109.6 |
Cl11—Nb4—Nb6 | 53.36 (4) | O9—C17—H17B | 109.6 |
Cl6—Nb4—Nb6 | 96.51 (4) | C18—C17—H17B | 109.6 |
Cl7—Nb4—Nb6 | 96.41 (4) | H17A—C17—H17B | 108.1 |
Nb5—Nb4—Nb6 | 60.47 (2) | C17—C18—C19 | 106.1 (9) |
Nb3—Nb4—Nb6 | 60.50 (2) | C17—C18—H18A | 110.5 |
O3—Nb4—Nb1 | 134.9 (1) | C19—C18—H18A | 110.5 |
Cl3—Nb4—Nb1 | 53.33 (4) | C17—C18—H18B | 110.5 |
Cl11—Nb4—Nb1 | 145.08 (4) | C19—C18—H18B | 110.5 |
Cl6—Nb4—Nb1 | 95.94 (4) | H18A—C18—H18B | 108.7 |
Cl7—Nb4—Nb1 | 96.49 (4) | C20—C19—C18 | 104.3 (9) |
Nb5—Nb4—Nb1 | 60.50 (2) | C20—C19—H19A | 110.9 |
Nb3—Nb4—Nb1 | 60.44 (2) | C18—C19—H19A | 110.9 |
Nb6—Nb4—Nb1 | 91.72 (2) | C20—C19—H19B | 110.9 |
O4—Nb5—Cl4 | 80.6 (1) | C18—C19—H19B | 110.9 |
O4—Nb5—Cl12 | 81.0 (1) | H19A—C19—H19B | 108.9 |
Cl4—Nb5—Cl12 | 161.67 (6) | O9—C20—C19 | 106.4 (9) |
O4—Nb5—Cl7 | 81.0 (1) | O9—C20—H20A | 110.5 |
Cl4—Nb5—Cl7 | 89.82 (6) | C19—C20—H20A | 110.5 |
Cl12—Nb5—Cl7 | 87.28 (6) | O9—C20—H20B | 110.5 |
O4—Nb5—Cl8 | 80.9 (1) | C19—C20—H20B | 110.5 |
Cl4—Nb5—Cl8 | 88.27 (6) | H20A—C20—H20B | 108.7 |
Cl12—Nb5—Cl8 | 88.88 (6) | C21—O10—C24 | 107.8 (8) |
Cl7—Nb5—Cl8 | 161.88 (6) | O10—C21—C22 | 108.4 (9) |
O4—Nb5—Nb4 | 135.1 (1) | O10—C21—H21A | 110.0 |
Cl4—Nb5—Nb4 | 97.38 (4) | C22—C21—H21A | 110.0 |
Cl12—Nb5—Nb4 | 95.53 (4) | O10—C21—H21B | 110.0 |
Cl7—Nb5—Nb4 | 54.06 (4) | C22—C21—H21B | 110.0 |
Cl8—Nb5—Nb4 | 144.02 (4) | H21A—C21—H21B | 108.4 |
O4—Nb5—Nb2 | 134.9 (1) | C21—C22—C23 | 103 (1) |
Cl4—Nb5—Nb2 | 95.66 (4) | C21—C22—H22A | 111.1 |
Cl12—Nb5—Nb2 | 97.30 (4) | C23—C22—H22A | 111.1 |
Cl7—Nb5—Nb2 | 144.04 (4) | C21—C22—H22B | 111.1 |
Cl8—Nb5—Nb2 | 54.06 (4) | C23—C22—H22B | 111.1 |
Nb4—Nb5—Nb2 | 89.97 (2) | H22A—C22—H22B | 109.1 |
O4—Nb5—Nb6 | 134.3 (1) | C24—C23—C22 | 102.7 (9) |
Cl4—Nb5—Nb6 | 145.07 (4) | C24—C23—H23A | 111.2 |
Cl12—Nb5—Nb6 | 53.26 (4) | C22—C23—H23A | 111.2 |
Cl7—Nb5—Nb6 | 96.28 (4) | C24—C23—H23B | 111.2 |
Cl8—Nb5—Nb6 | 95.58 (4) | C22—C23—H23B | 111.2 |
Nb4—Nb5—Nb6 | 60.51 (2) | H23A—C23—H23B | 109.1 |
Nb2—Nb5—Nb6 | 60.45 (2) | O10—C24—C23 | 104.3 (8) |
O4—Nb5—Nb1 | 134.0 (1) | O10—C24—H24A | 110.9 |
Cl4—Nb5—Nb1 | 53.35 (4) | C23—C24—H24A | 110.9 |
Cl12—Nb5—Nb1 | 144.97 (4) | O10—C24—H24B | 110.9 |
Cl7—Nb5—Nb1 | 96.31 (4) | C23—C24—H24B | 110.9 |
Cl8—Nb5—Nb1 | 96.97 (4) | H24A—C24—H24B | 108.9 |
Nb4—Nb5—Nb1 | 60.50 (2) | C25—O11—C28 | 109.1 (7) |
Nb2—Nb5—Nb1 | 60.53 (2) | O11—C25—C26 | 106.8 (8) |
Nb6—Nb5—Nb1 | 91.75 (2) | O11—C25—H25A | 110.4 |
Cl12—Nb6—Cl9 | 89.46 (6) | C26—C25—H25A | 110.4 |
Cl12—Nb6—Cl11 | 88.43 (6) | O11—C25—H25B | 110.4 |
Cl9—Nb6—Cl11 | 164.93 (6) | C26—C25—H25B | 110.4 |
Cl12—Nb6—Cl10 | 164.84 (6) | H25A—C25—H25B | 108.6 |
Cl9—Nb6—Cl10 | 89.32 (5) | C27—C26—C25 | 110 (1) |
Cl11—Nb6—Cl10 | 88.82 (5) | C27—C26—H26A | 109.8 |
Cl12—Nb6—Nb5 | 53.44 (4) | C25—C26—H26A | 109.8 |
Cl9—Nb6—Nb5 | 94.80 (4) | C27—C26—H26B | 109.8 |
Cl11—Nb6—Nb5 | 95.91 (4) | C25—C26—H26B | 109.8 |
Cl10—Nb6—Nb5 | 141.71 (4) | H26A—C26—H26B | 108.2 |
Cl12—Nb6—Nb4 | 94.55 (4) | C26—C27—C28 | 107.9 (9) |
Cl9—Nb6—Nb4 | 141.64 (4) | C26—C27—H27A | 110.1 |
Cl11—Nb6—Nb4 | 53.42 (4) | C28—C27—H27A | 110.1 |
Cl10—Nb6—Nb4 | 95.77 (4) | C26—C27—H27B | 110.1 |
Nb5—Nb6—Nb4 | 59.02 (2) | C28—C27—H27B | 110.1 |
Cl12—Nb6—Nb2 | 96.47 (4) | H27A—C27—H27B | 108.4 |
Cl9—Nb6—Nb2 | 53.27 (4) | O11—C28—C27 | 105.9 (7) |
Cl11—Nb6—Nb2 | 141.81 (4) | O11—C28—H28A | 110.6 |
Cl10—Nb6—Nb2 | 94.90 (4) | C27—C28—H28A | 110.6 |
Nb5—Nb6—Nb2 | 59.19 (2) | O11—C28—H28B | 110.6 |
Nb4—Nb6—Nb2 | 88.39 (2) | C27—C28—H28B | 110.6 |
Cl12—Nb6—Nb3 | 141.76 (4) | H28A—C28—H28B | 108.7 |
Cl9—Nb6—Nb3 | 95.75 (4) | C32—O12—C29 | 110.4 (6) |
Cl11—Nb6—Nb3 | 95.13 (4) | O12—C29—C30 | 103.7 (7) |
Cl10—Nb6—Nb3 | 53.38 (4) | O12—C29—H29A | 111.0 |
Nb5—Nb6—Nb3 | 88.34 (2) | C30—C29—H29A | 111.0 |
Nb4—Nb6—Nb3 | 59.19 (2) | O12—C29—H29B | 111.0 |
Nb2—Nb6—Nb3 | 58.81 (2) | C30—C29—H29B | 111.0 |
Cl12—Nb6—I2 | 81.77 (4) | H29A—C29—H29B | 109.0 |
Cl9—Nb6—I2 | 82.38 (4) | C31—C30—C29 | 101.6 (6) |
Cl11—Nb6—I2 | 82.55 (4) | C31—C30—H30A | 111.5 |
Cl10—Nb6—I2 | 83.09 (4) | C29—C30—H30A | 111.5 |
Nb5—Nb6—I2 | 135.19 (2) | C31—C30—H30B | 111.5 |
Nb4—Nb6—I2 | 135.95 (2) | C29—C30—H30B | 111.5 |
Nb2—Nb6—I2 | 135.65 (2) | H30A—C30—H30B | 109.3 |
Nb3—Nb6—I2 | 136.47 (2) | C30—C31—C32 | 104.3 (6) |
Nb1—Cl1—Nb2 | 73.50 (5) | C30—C31—H31A | 110.9 |
Nb1—Cl2—Nb3 | 73.21 (4) | C32—C31—H31A | 110.9 |
Nb1—Cl3—Nb4 | 73.26 (5) | C30—C31—H31B | 110.9 |
Nb5—Cl4—Nb1 | 73.48 (5) | C32—C31—H31B | 110.9 |
Nb2—Cl5—Nb3 | 71.81 (4) | H31A—C31—H31B | 108.9 |
Nb4—Cl6—Nb3 | 72.03 (4) | O12—C32—C31 | 106.1 (6) |
Nb4—Cl7—Nb5 | 71.63 (4) | O12—C32—H32A | 110.5 |
Nb2—Cl8—Nb5 | 71.77 (4) | C31—C32—H32A | 110.5 |
Nb2—Cl9—Nb6 | 73.44 (5) | O12—C32—H32B | 110.5 |
Nb6—Cl10—Nb3 | 73.34 (4) | C31—C32—H32B | 110.5 |
Nb6—Cl11—Nb4 | 73.21 (4) | H32A—C32—H32B | 108.7 |
Nb6—Cl12—Nb5 | 73.30 (4) | ||
C4—O5—C1—C2 | 14.9 (9) | C20—O9—C17—C18 | 10 (2) |
O5—C1—C2—C3 | −29.6 (9) | O9—C17—C18—C19 | 3 (2) |
C1—C2—C3—C4 | 32.4 (8) | C17—C18—C19—C20 | −13 (2) |
C1—O5—C4—C3 | 6.3 (9) | C17—O9—C20—C19 | −18 (2) |
C2—C3—C4—O5 | −24.3 (8) | C18—C19—C20—O9 | 18 (2) |
C8A_a—O6A_a—C5A_a—C6A_a | −30 (3) | C24—O10—C21—C22 | 3 (2) |
O6A_a—C5A_a—C6A_a—C7A_a | 45 (5) | O10—C21—C22—C23 | −24 (2) |
C5A_a—C6A_a—C7A_a—C8A_a | −41 (5) | C21—C22—C23—C24 | 36 (2) |
C5A_a—O6A_a—C8A_a—C7A_a | 7 (4) | C21—O10—C24—C23 | 20 (1) |
C6A_a—C7A_a—C8A_a—O6A_a | 21 (5) | C22—C23—C24—O10 | −34 (1) |
O6B_b—C5B_b—C6B_b—C7B_b | −32 (10) | C28—O11—C25—C26 | 6 (1) |
C12—O7—C9—C10 | 20 (1) | O11—C25—C26—C27 | −9 (2) |
O7—C9—C10—C11 | 4 (1) | C25—C26—C27—C28 | 8 (2) |
C9—C10—C11—C12 | −25 (1) | C25—O11—C28—C27 | −1 (1) |
C9—O7—C12—C11 | −35 (1) | C26—C27—C28—O11 | −5 (2) |
C10—C11—C12—O7 | 36 (1) | C32—O12—C29—C30 | 27 (1) |
C16—O8—C13—C14 | 12.1 (8) | O12—C29—C30—C31 | −36.7 (8) |
O8—C13—C14—C15 | −31.5 (8) | C29—C30—C31—C32 | 33.1 (8) |
C13—C14—C15—C16 | 38.1 (8) | C29—O12—C32—C31 | −6 (1) |
C13—O8—C16—C15 | 12.5 (9) | C30—C31—C32—O12 | −17.8 (9) |
C14—C15—C16—O8 | −31.7 (9) |