Bruker APEXII CCD diffractometer | 1786 independent reflections |
Radiation source: Incoatec IMuS microfocus Cu tube | 1770 reflections with I > 2σ(I) |
Multi-layer optics monochromator | Rint = 0.019 |
φ and ω scans | θmax = 72.4°, θmin = 4.1° |
Absorption correction: multi-scan (AXScale; Bruker, 2016) | h = −29→26 |
Tmin = 0.684, Tmax = 0.754 | k = −7→7 |
15813 measured reflections | l = −16→16 |