Table 2. Experimental details.
| Crystal data | |
| Chemical formula | C26H22O6 |
| M r | 430.43 |
| Crystal system, space group | Monoclinic, P21/c |
| Temperature (K) | 100 |
| a, b, c (Å) | 6.1631 (6), 19.253 (2), 18.0743 (19) |
| β (°) | 96.830 (1) |
| V (Å3) | 2129.5 (4) |
| Z | 4 |
| Radiation type | Mo Kα |
| μ (mm−1) | 0.10 |
| Crystal size (mm) | 0.4 × 0.12 × 0.06 |
| Data collection | |
| Diffractometer | Bruker SMART APEX CCD area detector |
| Absorption correction | Multi-scan (SADABS; Bruker, 2004 ▸) |
| T min, T max | 0.964, 1.00 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 19788, 5132, 4358 |
| R int | 0.021 |
| (sin θ/λ)max (Å−1) | 0.667 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.048, 0.125, 1.02 |
| No. of reflections | 5132 |
| No. of parameters | 292 |
| H-atom treatment | H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) | 0.42, −0.23 |