Table 2. Experimental details.
| Crystal data | |
| Chemical formula | C32H24 |
| M r | 408.51 |
| Crystal system, space group | Monoclinic, P21/c |
| Temperature (K) | 193 |
| a, b, c (Å) | 9.3106 (11), 8.7232 (8), 13.4776 (12) |
| β (°) | 91.959 (8) |
| V (Å3) | 1093.99 (19) |
| Z | 2 |
| Radiation type | Mo Kα |
| μ (mm−1) | 0.07 |
| Crystal size (mm) | 0.40 × 0.32 × 0.17 |
| Data collection | |
| Diffractometer | Stoe IPDS 2T |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 5905, 2604, 1416 |
| R int | 0.051 |
| (sin θ/λ)max (Å−1) | 0.661 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.061, 0.196, 0.97 |
| No. of reflections | 2604 |
| No. of parameters | 145 |
| H-atom treatment | H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) | 0.19, −0.22 |