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. 2020 Mar 5;5(Pt 3):x200307. doi: 10.1107/S2414314620003077

Table 2. Experimental details.

Crystal data
Chemical formula C32H24
M r 408.51
Crystal system, space group Monoclinic, P21/c
Temperature (K) 193
a, b, c (Å) 9.3106 (11), 8.7232 (8), 13.4776 (12)
β (°) 91.959 (8)
V3) 1093.99 (19)
Z 2
Radiation type Mo Kα
μ (mm−1) 0.07
Crystal size (mm) 0.40 × 0.32 × 0.17
 
Data collection
Diffractometer Stoe IPDS 2T
No. of measured, independent and observed [I > 2σ(I)] reflections 5905, 2604, 1416
R int 0.051
(sin θ/λ)max−1) 0.661
 
Refinement
R[F 2 > 2σ(F 2)], wR(F 2), S 0.061, 0.196, 0.97
No. of reflections 2604
No. of parameters 145
H-atom treatment H-atom parameters constrained
Δρmax, Δρmin (e Å−3) 0.19, −0.22

Computer programs: X-AREA and X-RED (Stoe & Cie, 1996), SIR2004 (Burla et al., 2005), SHELXL2018/3 (Sheldrick, 2015) and PLATON (Spek, 2020).