Stoe Stadivari diffractometer | 1106 independent reflections |
Radiation source: Sealed X-ray tube, Axo Astix-f Microfocus source | 930 reflections with I > 2σ(I) |
Graded multilayer mirror monochromator | Rint = 0.061 |
Detector resolution: 5.81 pixels mm-1 | θmax = 27.5°, θmin = 2.6° |
ω scans | h = −14→14 |
Absorption correction: multi-scan (X-RED32; Stoe & Cie, 2019) | k = −14→14 |
Tmin = 0.410, Tmax = 1.000 | l = −9→9 |
26907 measured reflections |