| Rigaku Xcalibur, Sapphire3 diffractometer | 4779 independent reflections |
| Radiation source: fine-focus sealed X-ray tube, Enhance (Mo) X-ray Source | 3869 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.031 |
| Detector resolution: 16.1790 pixels mm-1 | θmax = 33.6°, θmin = 4.3° |
| ω scans | h = −21→21 |
| Absorption correction: multi-scan (CrysAlisPro; Rigaku, 2018) | k = −21→21 |
| Tmin = 0.922, Tmax = 1.000 | l = −20→19 |
| 31103 measured reflections |
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