| Crystal data |
| Chemical formula |
[Pt(C4N2S2)2(NH3)2] |
|
M
r
|
509.52 |
| Crystal system, space group |
Monoclinic, P21/c
|
| Temperature (K) |
100 |
|
a, b, c (Å) |
6.1778 (3), 7.7700 (4), 14.8862 (7) |
| β (°) |
95.935 (4) |
|
V (Å3) |
710.73 (6) |
|
Z
|
2 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
10.45 |
| Crystal size (mm) |
0.05 × 0.02 × 0.01 |
| |
| Data collection |
| Diffractometer |
Rigaku XtaLAB Synergy, Dualflex, HyPix |
| Absorption correction |
Multi-scan (CrysAlis PRO; Rigaku OD, 2019 ▸) |
|
T
min, T
max
|
0.509, 1.000 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
8027, 1556, 1375 |
|
R
int
|
0.034 |
| (sin θ/λ)max (Å−1) |
0.641 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.017, 0.038, 1.05 |
| No. of reflections |
1556 |
| No. of parameters |
89 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
0.62, −0.54 |
