STOE IPDS 2T diffractometer | 2784 reflections with I > 2σ(I) |
Radiation source: sealed X-ray tube, 12 x 0.4 mm long-fine focus | Rint = 0.036 |
Detector resolution: 6.67 pixels mm-1 | θmax = 28.0°, θmin = 2.6° |
rotation method, ω scans | h = −16→17 |
8583 measured reflections | k = −12→12 |
4123 independent reflections | l = −19→19 |