Table 2. Experimental details.
| Crystal data | |
| Chemical formula | C19H24O5 |
| M r | 332.38 |
| Crystal system, space group | Monoclinic, P21/c |
| Temperature (K) | 120 |
| a, b, c (Å) | 13.1494 (10), 9.6899 (6), 14.8185 (13) |
| β (°) | 113.295 (6) |
| V (Å3) | 1734.2 (2) |
| Z | 4 |
| Radiation type | Mo Kα |
| μ (mm−1) | 0.09 |
| Crystal size (mm) | 0.22 × 0.11 × 0.06 |
| Data collection | |
| Diffractometer | Stoe IPDS 2T |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 8583, 4123, 2784 |
| R int | 0.036 |
| (sin θ/λ)max (Å−1) | 0.659 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.072, 0.185, 1.05 |
| No. of reflections | 4123 |
| No. of parameters | 222 |
| H-atom treatment | H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) | 0.24, −0.30 |