| Crystal data |
| Chemical formula |
[Pd(NO3)(C15H11N3)]NO3
|
|
M
r
|
463.69 |
| Crystal system, space group |
Orthorhombic, P
n
a21
|
| Temperature (K) |
223 |
|
a, b, c (Å) |
6.2190 (2), 33.9728 (15), 7.4819 (3) |
|
V (Å3) |
1580.75 (11) |
|
Z
|
4 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
1.22 |
| Crystal size (mm) |
0.21 × 0.14 × 0.06 |
| |
| Data collection |
| Diffractometer |
PHOTON 100 CMOS detector |
| Absorption correction |
Multi-scan (SADABS; Bruker, 2016 ▸) |
|
T
min, T
max
|
0.688, 0.745 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
41749, 3116, 2745 |
|
R
int
|
0.084 |
| (sin θ/λ)max (Å−1) |
0.618 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.027, 0.048, 1.09 |
| No. of reflections |
3116 |
| No. of parameters |
244 |
| No. of restraints |
1 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
0.34, −0.43 |
| Absolute structure |
Flack x determined using 1141 quotients [(I
+)−(I
−)]/[(I
+)+(I
−)] Parsons et al. (2013 ▸). |
| Absolute structure parameter |
0.006 (16) |
