| Crystal data |
| Chemical formula |
[RuCl2(C10H14)(C21H21O3P)] |
|
M
r
|
658.53 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
100 |
|
a, b, c (Å) |
12.4069 (17), 14.0221 (19), 16.934 (2) |
| α, β, γ (°) |
91.459 (3), 91.205 (3), 90.613 (3) |
|
V (Å3) |
2944.2 (7) |
|
Z
|
4 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
0.80 |
| Crystal size (mm) |
0.58 × 0.28 × 0.21 |
| |
| Data collection |
| Diffractometer |
Bruker APEX DUO 4K-CCD |
| Absorption correction |
Multi-scan SADABS (Bruker, 2008 ▸) |
|
T
min, T
max
|
0.654, 0.850 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
88599, 14838, 13368 |
|
R
int
|
0.053 |
| (sin θ/λ)max (Å−1) |
0.674 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.070, 0.181, 1.09 |
| No. of reflections |
14838 |
| No. of parameters |
698 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
3.95, −1.95 |
