| Enraf–Nonius CAD-4 diffractometer | 9324 independent reflections |
| Radiation source: fine-focus sealed tube | 4039 reflections with I > 2σ(I) |
| Detector resolution: 28.5714 pixels mm-1 | Rint = 0.160 |
| ω scans | θmax = 25.4°, θmin = 1.1° |
| Absorption correction: ψ scan (North et al., 1968) | h = 0→22 |
| Tmin = 0.97, Tmax = 0.98 | k = 0→12 |
| 9324 measured reflections | l = −33→32 |
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