| Bruker APEXII CCD diffractometer | 10556 reflections with I > 2σ(I) |
| φ and ω scans | Rint = 0.035 |
| Absorption correction: multi-scan (SADABS; Krause et al., 2015) | θmax = 36.4°, θmin = 1.7° |
| Tmin = 0.676, Tmax = 0.747 | h = −13→13 |
| 82074 measured reflections | k = −20→20 |
| 11855 independent reflections | l = −21→21 |