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. 2021 Mar 2;13(2):157–166. doi: 10.1016/j.chmed.2021.01.005

Table 9.

1H NMR chemical shift of biphenyclooctene lignans.

Positions Chemical shift
H4, H11 5.9–7.0
H7, H8 1.7–2.8
H6, H9 Without substituents 2.0–2.7
Oxygen-containing substituents 4.0–6.0
OCH3 3.2–3.9
OCH2O 5.6–6.0
Cyclooctent moiety methyl proton C7 is substituted for OH H17 (1.1–1.4)
H18 (1.3–1.4)
H17, H18 C7 only has methyl substitution H17,18 (0.6–1.1)