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. 2022 Aug 28;55(17):7380–7391. doi: 10.1021/acs.macromol.2c01071

Figure 3.

Figure 3

(a) Conversion vs time curve and corresponding semilogarithmic plot determined by 1H NMR spectroscopy for the RAFT aqueous dispersion polymerization of DMAC at 30 °C in 2.0 M ammonium sulfate when targeting a PDMAC DP of 5000 at 20% w/w solids. (b) Aqueous GPC curves obtained by periodic sampling of the reaction mixture to monitor the evolution in the molecular weight distribution (see Figure S3 for the corresponding normalized GPC curves).