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. 2022 Mar 9;9(9):nwac045. doi: 10.1093/nsr/nwac045

Figure 4.

Figure 4.

Acceleration processes using Fenton's reagent. (A--C) Crystallization processes of silicalite-1 at 343 K under (A) Fenton conditions, (B) ultraviolet (UV) conditions (4.0 mW/cm2) and (C) dark conditions. (D--F) Electron paramagnetic resonance (EPR) spectra of the TPAOH–TEOS–H2O system under (D) Fenton conditions, (E) UV conditions (4.0 mW/cm2) and (F) dark conditions. The EPR signals are marked by the following: red circles, •OH; green rectangles, oxidized DMPO radicals; blue arrows, silicon-based radicals; asterisks, ethanol radicals; and red rectangles, oxidized BMPO radicals. Reprinted with permission from ref. [75].