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. 2022 Jan 19;414(25):7461–7472. doi: 10.1007/s00216-022-03881-3

Table 2.

Assay range, accuracy, and precision of inter-day validation runs for targeted analytes

Range (nmol/L) Accuracy (RSD, %) Precision (relative error, %)
LLOQ ULOQ High Mid Low LLOQ High Mid Low LLOQ
11-Deoxycorticosterone 0.092 189 5.7 4.7 5.7 10.1  − 1.2  − 0.2 0.9 0.3
11-Deoxycortisol 0.088 180 5.2 6.4 5.8 7.2  − 1.3  − 4.8  − 1.5  − 1.9
17α-Hydroxyprogesterone 0.092 189 6.9 8.9 5.7 9.6  − 1.9  − 1.2 0.2  − 5.7
21-Deoxycortisol 0.088 180 7.9 7.3 6.3 16.3  − 3.5  − 2.6 2.2  − 6.2
5α-Dihydrotestosterone 0.105 215 6.4 5.9 8.1 9.6  − 0.6  − 1.9 5.7  − 8.4
Aldosterone 0.085 173 14.9 6.7 9.7 10.3 9.5 3.9 3.3 3.1
Androstenedione 0.107 218 5.4 5.2 6.9 7.7  − 4.8 0.1  − 2.0 6.9
Androsterone 0.420 861 9.3 9.4 8.2 10.5  − 7.0  − 3.7 2.7 8.4
Corticosterone 0.705 1443 5.1 7.0 5.3 7.6 0.2 -3.3 2.3 9.8
Cortisol 0.378 8967 8.3 10.3 7.6 14.6 2.2 0.9  − 1.9 5.6
Cortisone 0.177 1387 5.9 5.6 5.2 4.6  − 0.2  − 2.9 0.9 5.5
DHEA 0.846 867 10.8 8.0 12.8 16.6 0.1  − 1.4 2.7 9.6
DHEA-S 6.252 12,805 8.8 7.4 7.5 7.0 2.1 7.4 4.3 4.6
Etiocholanolone 0.210 215 6.5 6.0 6.1 16.6  − 3.7 0.0 1.9 0.6
Pregnenolone 0.771 790 5.5 6.1 9.3 8.5  − 0.2  − 5.9 7.7  − 5.9
Progesterone 0.476 1590 6.2 5.2 4.5 6.3 0.3  − 2.2 1.7 2.9
Testosterone 0.105 867 6.2 6.2 5.8 7.4  − 3.2  − 3.8  − 1.1 3.9