Table 1.
X-ray data collection and refinement statistics
| Dataset | |
|---|---|
| Data collection | |
| Resolution rang (Å) | 63.04–2.64 (2.734–2.64) |
| Wavelength (Å) | 0.9792 |
| Total Reflection | 56,873 (5599) |
| Space group | P 21 21 21 |
| Cell dimensions | |
| a, b, c (Å) | 73.65, 126.09, 207.09 |
| α, β, γ (°) | 90.0, 90.0, 90.0 |
| Rmerge | 0.102 (1.19) |
| CC1/2 | 0.999 (0.836) |
| I/σ(I) | 18.3 (2.2) |
| Completeness (%) | 99.1 (99.4) |
| Multiplicity | 13.3 (13.8) |
| Refinement | |
| Resolution (Å) | |
| Rwork (%) | 23.35 (34.68) |
| Rfree (%) | 28.07 (41.21) |
| Ramachandran plot (%) | |
| Ramachandran favored (%) | 96.13 |
| Ramachandran allowed (%) | 3.87 |
| Ramachandran outliers (%) | 0.00 |
One crystal was used for determination of each structure. Values in parentheses are for highest resolution shell.