Table 3.
Cryogel | Molar Ratio | Charged Amount | |||
---|---|---|---|---|---|
PA:ANI | ANI:AAm | ANI | PA | APS | |
1-1 | 1:5 | 1:2.4 | 2.5 mmol | 0.50 mmol | 0.63 mmol |
1-2 | 1:2 | 3.0 mmol | 0.60 mmol | 0.76 mmol | |
1-3 | 2:3 | 4.0 mmol | 0.80 mmol | 1.000 mol | |
2-1 | 1:4 | 1:2.4 | 2.5 mmol | 0.63 mmol | 0.63 mmol |
2-2 | 1:2 | 3.0 mmol | 0.75 mmol | 0.76 mmol | |
2-3 | 2:3 | 4.0 mmol | 1.00 mmol | 1.00 mmol | |
3-1 | 1:3 | 1:2.4 | 2.5 mmol | 0.83 mmol | 0.63 mmol |
3-2 | 1:2 | 3.0 mmol | 1.00 mmol | 0.76 mmol | |
3-3 | 2:3 | 4.0 mmol | 1.33 mmol | 1.00 mmol |
a AAm (6 mmol), MBA (0.075 mmol), KPS (0.03 mmol) and VC (0.035 mmol) were added. The total amount of water was 2.0 mL.