. 2022 Sep 22;3(4):101700. doi: 10.1016/j.xpro.2022.101700

Table 1.

Quantification of reagents, solvent, and product

Reagent	Mw (g/mol)	m (g)	n (mmol)	Equiv.	V (mL)	Conc (M)	Density (g/mL)	Yield (%)
4-Fluoro-3-iodonitrobenzene	267	5.6	21.0	1.0
Benzene	78		23.0	1.1	2.1		0.87
m-CPBA (80%)	173	5.0	23.0	1.1
TfOH	150		42.0	2.0	3.7		1.67
DCM					105	0.2
1a^a	493	9.2	18.7					89

The product is benchtop stable. Can be stored at 20°C–25°C without any precautions to avoid moist and/or air.