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Quantification of reagents, solvent, and product
| Reagent | Mw (g/mol) | m (mg) | n (mmol) | Equiv. | V (mL) | Conc (M) | Density (g/mL) | Yield (%) |
|---|---|---|---|---|---|---|---|---|
| 1b | 527 | 105 | 0.2 | 1.0 | ||||
| H2O | 135 | 0.2 | 1.1 | 0.004 | 0.99 | |||
| Cs2CO3 | 138 | 65 | 0.2 | 1.0 | ||||
| EtOAc | 1.0 | 0.2 | ||||||
| 4a | 375 | 68 | 0.181 | 91 |
aThe product is benchtop stable. Can be sto red at 20°C–25°C without any precautions to avoid moist and/or air.
