Official websites use .gov
A
.gov website belongs to an official
government organization in the United States.
Secure .gov websites use HTTPS
A lock (
) or https:// means you've safely
connected to the .gov website. Share sensitive
information only on official, secure websites.
Optimization of the reaction condition for the alcohol oxidation.
| Entry | B-V-PIL/W (mg) | Solvent | Temp. (°C) | Yield (%) |
|---|---|---|---|---|
| 1 | 10 | H2O | 60 | 30 |
| 2 | 10 | H2O:EtOH (2:1) | 60 | 40 |
| 3 | 20 | H2O:EtOH (2:1) | 60 | 50 |
| 4 | 30 | H2O:EtOH (2:1) | 60 | 60 |
| 5 | 40 | H2O:EtOH (2:1) | 60 | 75 |
| 6 | 50 | H2O:EtOH (2:1) | 60 | 75 |
| 7 | 40 | H2O:EtOH (2:1) | 70 | 95 |
| 8 | 40 | H2O:EtOH (2:1) | 80 | 90 |
