| Crystal data |
| Chemical formula |
[AuCl(C16H13PS)] |
|
M
r
|
500.71 |
| Crystal system, space group |
Orthorhombic, P212121
|
| Temperature (K) |
173 |
|
a, b, c (Å) |
10.0322 (13), 12.0784 (15), 12.9412 (16) |
|
V (Å3) |
1568.1 (3) |
|
Z
|
4 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
9.77 |
| Crystal size (mm) |
0.24 × 0.16 × 0.11 |
| |
| Data collection |
| Diffractometer |
Bruker APEXII CCD |
| Absorption correction |
Multi-scan (SADABS; Krause et al., 2015 ▸) |
|
T
min, T
max
|
0.474, 0.745 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
13335, 3075, 2854 |
|
R
int
|
0.037 |
| (sin θ/λ)max (Å−1) |
0.617 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.025, 0.059, 1.08 |
| No. of reflections |
3075 |
| No. of parameters |
341 |
| No. of restraints |
837 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
1.02, −0.53 |
| Absolute structure |
Flack x determined using 1149 quotients [(I
+)−(I
−)]/[(I
+)+(I
−)] (Parsons et al., 2013 ▸) |
| Absolute structure parameter |
−0.002 (6) |
