Table 2. Experimental details.
| Crystal data | |
| Chemical formula | C35H22ClNO7 |
| M r | 603.98 |
| Crystal system, space group | Triclinic, P
|
| Temperature (K) | 296 |
| a, b, c (Å) | 8.0202 (1), 9.8474 (2), 19.4712 (4) |
| α, β, γ (°) | 95.422 (1), 94.693 (1), 103.857 (1) |
| V (Å3) | 1477.66 (5) |
| Z | 2 |
| Radiation type | Mo Kα |
| μ (mm−1) | 0.18 |
| Crystal size (mm) | 0.19 × 0.18 × 0.16 |
| Data collection | |
| Diffractometer | Bruker SMART APEXII CCD |
| Absorption correction | Multi-scan (SADABS; Bruker, 2017 ▸) |
| T min, T max | 0.966, 0.971 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 25466, 5207, 4255 |
| R int | 0.024 |
| (sin θ/λ)max (Å−1) | 0.595 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.038, 0.114, 1.03 |
| No. of reflections | 5207 |
| No. of parameters | 410 |
| No. of restraints | 6 |
| H-atom treatment | H atoms treated by a mixture of independent and constrained refinement |
| Δρmax, Δρmin (e Å−3) | 0.26, −0.33 |