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Indole optimization.
|
| |||||
|---|---|---|---|---|---|
|
Entry |
Loading [mol %] |
Temperature [°C] |
Solvent |
Time [h] |
Yield[a] [%] |
|
1 |
5 |
80 |
1,2‐DCE |
1 |
84 |
|
2 |
5 |
40 |
HFIP |
1 |
80 |
|
3 |
1 |
40 |
HFIP |
1 |
89 |
[a] Isolated yield.
