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. 2022 Oct 11;60(1):1994–2001. doi: 10.1080/13880209.2022.2128825

Table 1.

Composition as volatile constituents and classes of substances of B. incana leaf hydroalcoholic extract.

Compound LRIa on DB-5ms LRIa on VF-WAXms Amountb Percentage
Sulphur compounds        
 Dimethyl disulphide 742 1080 3959 1.99
 Isobutyl isothiocyanate 929 1322 610 0.31
 Dimethyl trisulphide 969 1388 21,163 10.66
 3-Butenyl isothiocyanate 973 1462 85,532 43.10
 Methyl methylthiomethyl disulphide 1135 1665 520 0.26
 All     111,784 56.33
Nitriles        
 4-Pentenenitrile 745 1279 5254 2.65
 Heptanenitrile 991 1408 120 0.06
 All     5374 2.71
Aldehydes        
 (E)-2-Pentenal 758 1131 387 0.19
 Heptanal 904 1186 776 0.39
 (E)-2-Heptenal 958 1329 571 0.29
 Octanal 1004 1290 1116 0.56
 (E)-2-Octenal 1058 1433 140 0.07
 Nonanal 1105 1396 4201 2.12
 Decanal 1207 1501 7448 3.75
 Undecanal 1307 1606 240 0.12
 Dodecanal 1408 1711 1174 0.59
 Tridecanal 1510 1817 559 0.28
 Tetradecanal 1610 1922 1058 0.53
 β-Cyclocitral 1220 1624 1388 0.70
 Safranal 1200 1649 1071 0.54
 All     20,128 10.14
Ketones        
 6-Methyl-5-hepten-2-one 985 1340 249 0.13
 All     249 0.13
Alcohols        
 1-Hexanol 870 1347 188 0.09
 1-Octen-3-ol 980 1448 233 0.12
 2-Ethyl-1-hexanol 1028 1489 484 0.24
 (Z)-2-Octen-1-ol 1060 1620 356 0.18
 (E)-2-Octen-1-ol 1068 1616 101 0.05
 1-Octanol 1071 1557 171 0.09
 1-Nonanol 1173 1659 363 0.18
 Dodecanol 1475 1966 15,106 7.61
 Tetradecanol 1576 2171 5164 2.6
 All     22,165 11.17
Acids        
 Butanoic acid 779 1636 5276 2.66
 Hexanoic acid 978 1851 7856 3.96
 Octanoic acid 1171 2064 3707 1.87
 Hexadecanoic acid 1960 3000 2426 1.22
 All     19,264 9.71
Esters        
 3-Methyl-1-butyl acetate 876 1121 829 0.42
 Hexyl acetate 1011 1270 3001 1.51
 1-Methylbutyl butanoate 1015 1208 509 0.26
 Butyl hexanoate 1185 1412 664 0.33
 Hexyl butanoate 1194 1415 228 0.11
 Methyl hexadecanoate 1926 2216 3268 1.65
 All     8498 4.28
Terpenes        
 Limonene 1029 1193 4363 2.20
 (Z)-Calamenene 1531 1835 1335 0.67
 Guaiol 1597 2087 2333 1.18
 Bulnesol 1667 2208 2391 1.20
 All     10,423 5.25

aLinear retention indexes calculated according to the Van Den Dool and Kratz equation.

bPeak area arbitrary scale.