TABLE 1.
Determination of the best conditions such as the catalyst, amount of catalyst, and temperature for the synthesis of 7a.
| Entry | Catalyst | Temp. (°C) | Catalyst (g) | Time (h) | Yield % a |
|---|---|---|---|---|---|
| 1 | None | r.t | - | 10 | - |
| 2 | None | 100 | - | 8 | - |
| 3 | CdO-NPs | r.t | 0.01 | 4 | 45 |
| 4 | CdO-NPs | r.t | 0.015 | 3 | 58 |
| 5 | CdO-NPs | r.t | 0.02 | 3 | 65 |
| 6 | Fe3O4-MNPs | r.t | 0.015 | 3 | 35 |
| 7 | Ag NPs | r.t | 0.015 | 3 | 78 |
| 8 | MWCNT | r.t | 0.015 | 3 | 27 |
| 9 | CuO-NPs | r.t | 0.015 | 3 | 38 |
| 10 | Ag/Fe3O4/CdO | r.t | 0.015 | 3 | 80 |
| 11 | Fe3O4/CdO | r.t | 0.015 | 3 | 70 |
| 12 | Ag/CdO@ MWCNT | r.t | 0.015 | 3 | 78 |
| 13 | Fe3O4/CdO/MWCNT | r.t | 0.015 | 3 | 70 |
| 14 | CdO@ MWCNT | r.t | 0.015 | 3 | 68 |
| 15 | Ag/Fe3O4/MWCNT | r.t | 0.015 | 3 | 75 |
| 16 | Ag/Fe3O4/CdO@MWCNT | r.t | 0.015 | 3 | 87 |
| 17 | Ag/Fe 3 O 4 /CdO@MWCNT | r.t | 0.02 | 3 | 95 |
| 18 | Ag/Fe3O4/CdO@MWCNT | reflux | 0.02 | 3 | 95 |
| 18 | Ag/Fe3O4/CdO@MWCNT | r.t | 0.015 | 3 | 87 |
| 19 | Ag/Fe3O4/CdO@MWCNT | r.t | 0.025 | 3 | 95 |
Isolated yields. Bold indicates best condition for performing reactions.