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. 2022 Sep 21;10:949205. doi: 10.3389/fchem.2022.949205

TABLE 1.

Determination of the best conditions such as the catalyst, amount of catalyst, and temperature for the synthesis of 7a.

Entry Catalyst Temp. (°C) Catalyst (g) Time (h) Yield % a
1 None r.t - 10 -
2 None 100 - 8 -
3 CdO-NPs r.t 0.01 4 45
4 CdO-NPs r.t 0.015 3 58
5 CdO-NPs r.t 0.02 3 65
6 Fe3O4-MNPs r.t 0.015 3 35
7 Ag NPs r.t 0.015 3 78
8 MWCNT r.t 0.015 3 27
9 CuO-NPs r.t 0.015 3 38
10 Ag/Fe3O4/CdO r.t 0.015 3 80
11 Fe3O4/CdO r.t 0.015 3 70
12 Ag/CdO@ MWCNT r.t 0.015 3 78
13 Fe3O4/CdO/MWCNT r.t 0.015 3 70
14 CdO@ MWCNT r.t 0.015 3 68
15 Ag/Fe3O4/MWCNT r.t 0.015 3 75
16 Ag/Fe3O4/CdO@MWCNT r.t 0.015 3 87
17 Ag/Fe 3 O 4 /CdO@MWCNT r.t 0.02 3 95
18 Ag/Fe3O4/CdO@MWCNT reflux 0.02 3 95
18 Ag/Fe3O4/CdO@MWCNT r.t 0.015 3 87
19 Ag/Fe3O4/CdO@MWCNT r.t 0.025 3 95
a

Isolated yields. Bold indicates best condition for performing reactions.