Skip to main content
. 2022 Sep 20;11(19):2930. doi: 10.3390/foods11192930

Table A3.

Average recovery, inter-day precision, and intra-day precision of the 32 compounds in the beef, pork, chicken, tallow and lard samples.

Compounds Spiked
Level
(µg/kg)
Beef (n = 5) Pork (n = 5) Chicken (n = 5) Tallow (n = 5) Lard (n = 5)
Average
Recovery
(%)
Intra-day
RSD
(%)
Inter-Day
RSD
(%)
Average
Recovery
(%)
Intra-Day
RSD
(%)
Inter-Day
RSD
(%)
Average
Recovery
(%)
Intra-Day
RSD
(%)
Inter-Day
RSD
(%)
Average
Recovery
(%)
Intra-Day
RSD
(%)
Inter-Day
RSD
(%)
Average
Recovery
(%)
Intra-Day
RSD
(%)
Inter-Day
RSD
(%)
3,5-dichloroaniline 5 11.5 25.7 9.9 45.4 2.6 5.7 15.7 21.0 0.3 19.9 15.2 1.8 15.9 18.9 3.0
10 14.6 19.3 5.6 34.5 13.1 10.1 12.9 23.4 8.5 15.3 12.9 5.1 25.8 12.8 6.9
100 20.1 10.2 6.9 27.2 3.9 9.3 28.6 6.3 0.3 27.0 14.6 3.8 30.9 7.0 3.5
500 20.2 4.7 3.1 25.4 14.9 3.3 24.3 5.9 9.4 28.2 5.1 7.1 31.3 5.5 9.6
Alachlor 5 70.3 25.0 3.0 62.7 4.5 6.2 76.7 15.3 1.8 69.2 9.7 2.3 69.9 21.7 0.8
10 70.9 19.3 1.5 65.6 12.3 1.5 83.9 4.4 6.5 60.5 15.4 8.2 70.5 13.9 6.1
100 73.6 3.2 2.1 79.5 1.8 6.1 90.1 4.9 8.5 73.4 9.3 3.3 72.6 5.1 2.9
500 84.4 12.8 5.7 78.0 4.6 5.2 98.4 3.9 5.7 74.3 10.7 7.3 75.0 2.4 9.1
Atrazine 5 85.1 13.7 7.6 104.6 6.0 0.8 68.4 26.4 9.2 65.6 15.6 8.1 62.4 17.2 1.2
10 69.4 18.2 1.1 74.4 23.4 6.4 68.8 15.4 6.7 68.3 8.7 9.9 61.2 8.6 0.3
100 80.9 3.4 5.3 82.0 2.3 5.0 88.4 2.3 3.4 82.5 5.3 7.8 73.4 1.5 3.4
500 85.5 9.6 5.2 83.0 8.0 9.5 79.8 1.0 9.7 89.3 3.4 7.3 77.1 6.2 2.4
Chinomethionat 5 113.1 20.5 0.6 71.1 1.3 3.8 66.1 21.2 7.3 27.6 21.6 7.9 17.6 18.6 5.6
10 55.4 16.2 8.4 50.8 19.7 0.1 61.8 21.6 8.7 25.2 14.4 10.2 33.9 18.7 1.8
100 67.1 11.9 1.5 79.9 4.4 2.6 71.6 9.2 5.1 29.1 7.1 2.2 33.1 14.4 3.3
500 69.8 22.5 7.2 77.5 11.5 3.4 70.8 17.6 6.4 29.4 4.3 3.5 33.0 6.5 8.1
Chlorpropham 5 111.1 4.5 9.2 88.4 20.7 1.2 62.5 15.0 2.9 61.2 8.6 4.6 87.6 3.2 4.8
10 89.5 8.8 3.4 68.8 14.1 0.8 73.7 17.9 2.3 67.3 3.8 3.1 86.4 6.6 2.5
100 75.1 7.4 3.6 73.4 7.3 7.8 78.3 5.8 9.9 77.3 6.1 6.7 78.3 4.3 10.2
500 77.2 13.5 5.5 77.5 5.1 2.6 78.4 19.2 7.0 73.1 1.4 8.5 77.7 1.7 3.2
Cyanazine 5 105.9 9.4 8.5 87.8 11.7 1.0 64.0 22.0 1.4 64.5 2.9 3.6 65.5 8.3 6.7
10 87.5 9.4 2.3 75.8 25.7 3.7 75.0 19.7 4.3 68.6 1.5 4.7 74.5 16.4 7.3
100 90.4 0.8 2.2 88.7 3.7 3.5 91.8 3.0 9.4 80.9 8.6 2.4 89.8 4.7 1.7
500 90.4 11.1 8.5 92.8 5.5 9.8 89.3 10.0 7.9 84.5 5.6 5.3 91.7 1.5 9.4
Cyprodinil 5 63.1 19.5 2.7 71.2 1.4 1.7 66.7 3.7 6.2 31.1 17.1 3.0 27.2 25.6 1.3
10 62.5 7.7 8.6 62.5 14.3 4.5 73.0 12.1 9.9 12.3 16.7 2.0 43.7 4.3 2.6
100 70.8 3.6 4.7 70.0 2.3 3.0 77.7 1.2 2.8 33.7 15.4 7.2 53.4 3.6 2.0
500 75.7 4.6 10.0 73.0 4.4 7.7 73.8 5.0 3.4 29.8 5.2 1.3 55.7 3.3 4.4
Dichlorobenil 5 40.4 9.1 0.2 44.8 7.3 7.9 45.8 9.6 8.2 33.6 11.5 9.6 27.7 20.0 6.0
10 38.0 14.7 0.9 28.9 17.4 9.7 24.8 28.8 6.7 29.6 10.6 2.3 43.7 7.3 9.0
100 50.6 9.8 5.4 27.9 16.3 7.9 37.5 9.2 4.3 40.2 12.3 4.3 51.1 8.2 3.1
500 52.7 19.5 7.4 52.3 19.8 1.3 51.4 16.4 4.4 37.0 6.9 4.1 60.5 12.0 6.6
Difenoconazole 5 95.5 5.7 9.3 113.0 1.1 0.0 65.1 7.3 3.7 66.0 3.2 2.8 60.5 3.4 8.2
10 84.1 7.5 5.2 101.1 14.0 3.6 70.8 6.2 1.2 61.6 1.0 3.2 65.1 4.6 4.9
100 85.2 2.7 3.6 76.9 1.7 6.7 85.5 3.1 7.2 85.6 8.4 3.6 76.7 2.7 6.3
500 86.0 6.0 0.5 82.4 2.0 5.4 83.9 6.5 1.6 88.9 1.3 8.7 80.6 1.7 0.4
Diphenylamine 5 71.6 3.4 10.0 64.2 3.0 3.0 76.9 7.1 9.2 60.3 3.7 7.3 67.7 4.8 7.9
10 78.3 7.8 8.1 76.9 12.5 9.1 71.4 7.7 0.0 67.4 5.3 1.8 68.3 2.4 0.7
100 77.5 3.6 0.7 71.1 2.1 1.1 72.5 0.5 1.6 71.5 5.7 6.1 80.9 2.7 3.2
500 76.2 5.1 1.2 76.1 3.8 8.8 79.3 8.0 9.2 74.4 4.4 0.2 86.9 3.0 5.6
Epoxiconazole 5 94.5 10.4 0.5 94.2 3.4 8.0 60.4 7.4 4.8 68.4 6.5 2.2 71.6 3.4 6.6
10 83.1 7.6 0.0 78.9 21.1 2.5 68.9 8.6 8.4 62.7 1.9 9.0 80.3 2.8 1.1
100 82.7 3.0 7.1 83.4 2.4 4.3 85.6 3.0 3.2 80.9 9.7 3.7 82.3 2.5 6.7
500 86.3 8.3 6.1 86.0 4.5 4.3 83.6 6.5 8.0 88.0 0.3 1.0 85.2 3.8 4.5
Esfenvalerate 5 117.5 5.8 8.0 83.3 11.9 8.0 65.2 7.0 6.7 73.5 5.1 7.9 63.6 3.3 1.4
10 88.5 9.7 5.2 66.3 18.4 0.9 70.8 9.1 4.4 67.4 3.1 4.7 67.5 3.5 1.4
100 83.0 5.6 6.3 74.0 4.5 3.1 81.4 8.0 2.6 77.7 7.1 4.0 71.2 1.5 6.1
500 84.4 12.5 0.1 78.7 10.5 3.6 79.8 7.5 10.0 74.7 2.8 10.1 73.3 3.6 3.7
Fenamidone 5 88.9 11.9 4.0 82.9 7.8 5.2 63.6 3.3 2.3 79.3 5.6 4.0 86.0 5.6 6.1
10 78.9 9.7 0.5 73.6 21.8 9.7 69.1 10.7 1.9 74.7 1.5 0.2 90.3 2.0 6.0
100 84.3 3.1 4.6 83.3 1.9 8.8 88.5 1.9 3.0 87.3 9.9 7.7 96.0 2.1 1.9
500 88.6 6.5 9.0 86.0 3.4 9.2 84.1 4.0 7.8 84.9 1.3 0.1 99.9 2.9 1.4
Fenoxanil 5 120.8 12.4 10.0 115.7 9.0 5.7 135.8 12.4 8.1 60.1 16.9 10.0 132.3 19.6 9.5
10 135.4 11.9 1.9 49.5 3.3 0.5 132.3 11.5 0.6 64.6 11.8 7.6 121.5 17.0 6.6
100 91.3 9.2 9.3 71.8 21.4 6.4 106.0 10.7 3.9 60.2 1.9 7.4 71.9 15.9 0.3
500 81.9 26.7 0.6 87.5 26.2 8.7 122.6 13.2 4.0 69.0 11.8 5.5 78.6 2.9 9.4
Flumioxazin 5 117.6 5.6 9.5 115.7 13.3 8.3 69.6 13.0 3.4 84.9 16.5 7.7 86.7 7.1 7.9
10 119.1 10.3 2.1 91.0 21.8 7.3 77.1 19.3 7.9 76.9 11.5 1.2 82.2 10.7 7.3
100 100.8 5.4 3.0 86.6 2.3 1.5 90.9 5.0 8.8 85.5 8.5 1.8 83.6 0.6 0.4
500 96.1 15.7 6.6 91.6 10.6 3.1 91.6 12.2 9.3 82.5 3.3 8.8 86.9 3.7 4.5
Fluopyram 5 114.4 9.1 10.1 97.2 4.2 8.2 63.7 9.2 5.4 69.5 12.1 10.1 70.4 3.5 1.0
10 93.3 7.8 5.5 84.5 18.1 8.5 67.9 11.6 8.1 73.5 0.7 6.9 81.1 2.1 1.4
100 86.4 3.2 7.8 82.9 1.5 3.0 89.6 2.1 6.1 83.8 10.7 4.7 87.7 3.3 5.9
500 91.1 6.8 9.3 86.3 3.7 7.5 84.3 5.6 4.6 80.7 1.2 4.4 90.0 3.6 5.4
Flusilazole 5 90.3 9.8 2.6 93.7 3.5 8.1 62.0 16.1 0.5 61.1 8.8 7.3 67.5 9.2 3.1
10 85.5 18.1 2.5 81.4 19.5 4.7 66.6 12.5 2.7 60.7 3.1 8.6 74.9 5.9 4.7
100 85.9 3.1 7.0 86.2 0.4 6.9 88.7 2.8 5.4 74.1 12.6 5.5 86.3 3.0 7.7
500 90.3 7.7 8.4 89.0 3.6 6.7 84.1 5.4 4.9 72.5 0.7 1.8 89.5 3.2 8.5
Flutriafol 5 116.0 6.4 9.5 110.6 2.3 0.7 64.8 18.7 9.8 N.D. 8.0 N.D.
10 87.7 5.6 9.9 84.3 11.3 8.7 137.5 76.2 6.7 N.D. 1.1 N.D.
100 83.0 5.0 6.3 84.0 2.7 1.8 88.0 3.8 2.8 N.D. 0.3 N.D.
500 86.6 5.9 4.6 86.2 6.3 8.8 87.3 10.8 9.1 N.D. 8.6 N.D.
PAM 5 102.3 4.0 3.7 106.3 4.9 5.4 100.3 9.8 7.9 62.7 6.5 9.8 76.3 2.9 3.1
10 74.1 19.3 3.4 85.4 18.5 8.5 78.9 4.7 5.6 77.3 1.9 9.2 74.1 7.0 3.3
100 70.9 14.1 0.3 86.8 5.8 4.8 71.6 9.7 3.4 70.6 8.0 1.8 73.3 8.7 9.5
500 72.6 6.0 0.7 71.5 17.2 7.3 73.0 11.8 3.2 79.2 1.5 4.4 78.3 6.1 4.8
Pendimethalin 5 119.6 6.7 4.2 95.7 14.1 0.8 61.7 18.4 9.8 22.5 16.4 7.5 37.5 22.1 7.7
10 87.7 6.8 3.8 62.0 18.3 7.6 63.5 16.9 8.2 21.7 11.1 8.7 48.7 19.0 3.4
100 78.2 4.2 3.6 79.0 3.0 2.6 86.5 6.6 5.5 30.9 14.6 0.9 30.5 12.6 1.3
500 72.6 20.6 4.5 79.1 15.2 1.5 76.5 12.6 6.0 35.4 10.9 4.1 31.2 5.9 4.9
Pentachloroaniline 5 70.7 3.1 0.7 68.8 4.5 2.4 68.5 5.1 2.8 26.0 21.5 0.8 37.1 13.9 3.3
10 60.8 11.4 7.5 65.4 15.9 6.2 73.1 3.4 3.3 34.3 6.8 8.3 42.5 9.9 5.7
100 81.2 2.0 3.9 75.8 0.4 7.9 77.2 1.5 1.3 39.7 9.8 3.5 42.7 3.0 3.2
500 75.0 5.6 7.3 76.6 3.6 8.5 77.8 2.7 8.3 42.9 7.5 2.4 45.6 4.4 3.9
Penthiopyrad 5 104.4 3.7 9.0 93.1 1.3 1.2 69.5 18.7 9.9 68.8 12.8 2.2 65.5 3.1 1.9
10 83.3 9.8 7.8 77.1 17.5 9.8 79.7 6.9 3.7 70.0 2.3 5.4 79.7 4.9 4.4
100 89.2 2.8 3.9 83.1 1.6 3.5 89.5 1.8 1.9 88.9 10.4 3.5 88.1 3.1 3.9
500 92.2 7.6 2.0 84.8 3.5 3.4 84.9 5.4 7.9 83.5 3.8 2.1 91.1 0.6 8.3
Phthalide 5 103.4 14.0 3.9 109.8 16.6 4.3 65.2 13.9 0.4 70.0 10.4 0.3 62.1 9.9 3.6
10 104.3 8.2 6.9 72.5 16.0 6.2 74.5 21.6 3.6 73.6 4.9 5.0 70.3 9.1 4.9
100 88.2 5.3 6.6 71.8 5.8 8.5 81.4 7.4 3.6 88.9 7.0 4.2 83.1 5.6 7.9
500 95.3 15.9 2.1 80.8 14.6 2.7 84.5 13.1 4.8 81.4 1.4 5.0 86.6 5.0 8.1
Picoxystrobin 5 80.1 5.7 4.7 83.4 2.4 6.6 68.5 17.5 9.2 73.6 1.6 6.8 64.1 13.3 5.0
10 73.8 5.7 9.9 70.5 13.5 0.8 65.1 17.0 9.7 60.5 3.9 5.0 83.4 6.7 9.4
100 85.3 4.6 9.9 84.8 4.6 4.6 90.4 2.2 7.3 74.8 9.9 4.1 88.0 2.5 4.7
500 89.1 6.1 0.2 86.7 2.1 5.0 86.6 8.0 3.2 73.1 2.0 1.5 93.3 2.1 9.2
Propiconazole 5 102.1 7.5 10.2 68.8 2.7 10.0 63.1 6.3 4.5 60.9 12.8 8.0 66.4 6.6 2.7
10 85.7 4.3 0.2 70.3 14.9 9.8 63.1 13.1 7.7 60.6 3.1 9.1 67.8 2.6 9.4
100 80.6 4.2 7.7 77.9 1.6 3.2 87.8 2.0 5.8 86.0 8.3 6.4 80.6 3.6 3.8
500 86.2 5.3 7.2 76.8 2.6 8.5 82.8 6.5 1.7 88.7 1.7 6.6 84.0 3.5 7.3
Quintozene 5 111.3 10.1 4.1 63.8 2.0 0.9 64.4 11.9 4.8 N.D. 3.5 N.D.
10 89.5 4.2 0.8 63.1 27.8 0.6 68.3 20.6 9.4 N.D. 2.0 35.1 36.6 9.3
100 91.2 6.0 8.2 79.2 4.3 4.8 72.0 3.9 0.8 15.4 30.7 7.7 26.8 9.8 0.8
500 95.3 11.5 4.3 74.7 10.3 3.9 75.6 16.9 8.9 7.2 57.4 0.7 32.4 39.0 2.9
Simazine 5 82.1 14.0 4.2 64.9 0.9 9.4 69.3 2.0 6.8 71.9 24.3 2.6 70.4 9.9 4.9
10 78.8 13.5 4.6 60.1 12.3 5.0 73.9 15.9 0.0 75.9 5.8 6.9 79.5 4.2 0.1
100 81.7 3.2 10.1 80.9 5.7 8.2 86.9 4.7 9.4 88.2 8.0 9.7 74.8 3.2 0.7
500 84.1 7.9 4.7 81.9 1.0 9.9 83.7 5.0 6.7 82.2 6.9 3.9 80.9 7.0 5.5
Thifluzamide 5 115.3 6.1 8.2 98.2 7.6 7.1 65.2 7.4 8.5 60.5 9.0 9.2 66.8 10.5 3.6
10 111.7 8.1 3.8 81.8 27.1 0.1 71.1 9.1 9.8 70.1 4.2 1.4 80.7 1.7 1.5
100 96.0 6.1 6.8 84.4 2.1 0.4 88.9 3.7 0.8 80.7 10.7 8.1 88.3 4.5 1.0
500 100.6 9.2 4.0 87.8 5.4 1.9 83.8 3.8 0.5 85.3 1.6 9.3 90.4 2.2 1.8
Vinclozoline 5 69.3 9.4 6.0 69.7 2.2 7.8 69.3 11.8 1.4 80.0 9.1 1.2 64.4 9.8 3.4
10 69.7 2.4 6.4 77.3 17.9 4.7 65.2 19.0 3.0 65.1 14.4 7.9 63.9 4.2 2.2
100 76.3 2.3 2.6 76.9 1.5 0.5 85.6 1.7 5.3 71.2 9.6 1.7 76.7 3.0 0.1
500 85.6 5.2 5.3 78.0 1.9 6.8 80.1 8.5 0.4 72.3 9.4 5.9 82.0 5.0 6.0