Table 1.
Comp. | Structure | Yield | M.p. | Comp. | Structure | Yield | M.p. |
---|---|---|---|---|---|---|---|
5a | 57% | 252.3–254.1 °C | 5j | 94% | 265.2–266.9 °C | ||
5b | 46% | 272.5–273.8 °C | 5k | 88% | 233.7–235.6 °C | ||
5c | 49% | 274.9–276.9 °C | 5l | 54% | 258.4–260.2 °C | ||
5d | 82% | 286.3–288.1 °C | 5m | 82% | 250.4–251.8 °C | ||
5e | 58% | 245.9–247.8 °C | 7a | 82% | 251.8–252.6 °C | ||
5f | 85% | 283.3–284.8 °C | 7b | 40% | 258.3–259.8 °C | ||
5g | 48% | 281.1–283.3 °C | 7c | 55% | 245.6–247.2 °C | ||
5h | 80% | 248.3–250.2 °C | 7d | 83% | 231.1–232.6 °C | ||
5i | 79% | 249.7–251.5 °C | 7e | 95% | 195.6–197.1 °C |